Benzenamine, 4-fluoro-N-(1-phenylethylidene)-

Base Information

Chemical Name:Benzenamine, 4-fluoro-N-(1-phenylethylidene)-
CAS No.:591751-71-2
Molecular Formula:C14H12FN
Molecular Weight:213.254
Hs Code.:
DSSTox Substance ID:DTXSID70461947
Nikkaji Number:J1.932.333A,J3.341.477C

Synonyms:Benzenamine, 4-fluoro-N-(1-phenylethylidene)-;591751-71-2;SCHEMBL13440552;DTXSID70461947

Suppliers and Price of Benzenamine, 4-fluoro-N-(1-phenylethylidene)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of Benzenamine, 4-fluoro-N-(1-phenylethylidene)-

Chemical Property:

Melting Point:86-87 °C
Boiling Point:290.3±32.0 °C(Predicted)
PSA：12.36000
Density:1.02±0.1 g/cm3(Predicted)
LogP:3.96640
XLogP3:3.5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:213.095377549
Heavy Atom Count:16
Complexity:235

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(=NC1=CC=C(C=C1)F)C2=CC=CC=C2

Technology Process of Benzenamine, 4-fluoro-N-(1-phenylethylidene)-

There total 2 articles about Benzenamine, 4-fluoro-N-(1-phenylethylidene)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 536-74-3
phenylacetylene

: 371-40-4
4-fluoroaniline

: 591751-71-2
4-fluoro-N-(α-methylbenzylidene)aniline

Guidance literature:: With C₄₆H₇₀Br₄Hg₂N₂; In tetrahydrofuran; at 67 ℃; for 11h; regioselective reaction; Inert atmosphere; Schlenk technique;
DOI:10.1039/c7dt04589a

Reference yield: 70.0%

: 98-86-2
acetophenone

: 371-40-4
4-fluoroaniline

: 591751-71-2
4-fluoro-N-(α-methylbenzylidene)aniline

Guidance literature:: With toluene-4-sulfonic acid; In toluene; at 100 ℃; for 12h; Molecular sieve;
DOI:10.1039/c7nj03912c

Reference yield: 95.0%

: 591751-71-2
4-fluoro-N-(α-methylbenzylidene)aniline

: 4-fluoro-N-(1-phenylethyl)benzenamine

Guidance literature:: With bis(1,5-cyclooctadiene)diiridium(I) dichloride; (Sc,Sa)-PEAPhos-Me; hydrogen; potassium iodide; In dichloromethane; at 20 ℃; for 24h; under 45004.5 Torr; enantioselective reaction; Autoclave; Glovebox;
DOI:10.1039/c4ra16062b