Benzenesulfonic acid, 4-(diphenylphosphino)-

Base Information

• Chemical Name: Benzenesulfonic acid, 4-(diphenylphosphino)-
• CAS No.: 60421-69-4
• Molecular Formula: C18H15O3PS
• Molecular Weight: 342.34900
• DSSTox Substance ID: DTXSID90413948
• Nikkaji Number: J1.162.806K

Synonyms:60421-69-4;4-(diphenylphosphino)benzenesulfonic acid;Benzenesulfonic acid, 4-(diphenylphosphino)-;SCHEMBL718256;DTXSID90413948;4-(diphenylphosphaneyl)benzenesulfonic acid

Chemical Property of Benzenesulfonic acid, 4-(diphenylphosphino)-

Chemical Property:

• PSA: 76.34000
• LogP: 3.77230
• XLogP3: 3.4
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 4
• Exact Mass: 342.04795251
• Heavy Atom Count: 23
• Complexity: 435

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC=C(C=C1)P(C2=CC=CC=C2)C3=CC=C(C=C3)S(=O)(=O)O

Technology Process of Benzenesulfonic acid, 4-(diphenylphosphino)-

There total 1 articles about Benzenesulfonic acid, 4-(diphenylphosphino)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ HSO3C6H4PPh2 (60421-69-4)

Guidance literature:

Aus dem Na-Salz mit HCl;

DOI:10.1016/S0040-4039(00)99997-0

Reference yield: 59.0%

copper(l) iodide (7681-65-4) + HSO3C6H4PPh2 (60421-69-4) + 4-([2,2′:5′,2″-terthiophene]-5-ylethynyl)pyridine → C74H52Cu2I2N2O6P2S8

Guidance literature:

In dichloromethane; at 20 ℃; for 24h; Schlenk technique; Inert atmosphere;

DOI:10.1021/acs.inorgchem.8b01684

Reference yield:

N-hydroxy-succinimide-(2-iodo)acetate (39028-27-8) + C35H48N9O11Pol + HSO3C6H4PPh2 (60421-69-4) → C2F3O2(1-)*C52H61N9O15PS(1+)

Guidance literature:

N-hydroxy-succinimide-(2-iodo)acetate; C₃₅H₄₈N₉O₁₁Pol; solid phase reaction;

HSO₃C₆H₄PPh₂; solid phase reaction;

With chlorotriisopropylsilane; water; trifluoroacetic acid; solid phase reaction;

DOI:10.1021/ja104903x

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