1H-Isoindole-1,3(2H)-dione,2-(2-azidoethyl)-

Base Information

• Chemical Name: 1H-Isoindole-1,3(2H)-dione,2-(2-azidoethyl)-
• CAS No.: 30250-66-9
• Molecular Formula: C10H8 N4 O2
• Molecular Weight: 216.199
• Hs Code.: 2929909090
• Mol file: 30250-66-9.mol

Synonyms:Phthalimide,N-(2-azidoethyl)- (8CI); N-2-(Azidoethyl)phthalimide

Chemical Property of 1H-Isoindole-1,3(2H)-dione,2-(2-azidoethyl)-

Chemical Property:

• Melting Point: 58 °C
• Boiling Point: °Cat760mmHg
• Flash Point: °C
• PSA: 87.13000
• Density: g/cm³
• LogP: 0.98356

Purity/Quality:

2-(2-azidoethyl)-1H-isoindole-1,3(2H)-dione ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1H-Isoindole-1,3(2H)-dione,2-(2-azidoethyl)-

There total 4 articles about 1H-Isoindole-1,3(2H)-dione,2-(2-azidoethyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

2-(2-bromoethyl)isoindoline-1,3-dione (574-98-1) → 2-(2-azidoethyl)isoindoline-1,3-dione (30250-66-9)

Guidance literature:

With sodium azide; potassium iodide; In water; acetone; at 20 ℃; for 60h; Inert atmosphere;

DOI:10.1002/anie.201612193

Reference yield: 91.0%

N-(2-Hydroxyethyl)phthalimide (3891-07-4) → 2-(2-azidoethyl)isoindoline-1,3-dione (30250-66-9)

Guidance literature:

With sodium azide; triethylamine; tetra-(n-butyl)ammonium iodide; In N,N-dimethyl-formamide; for 5h; Heating;

DOI:10.1016/j.tetlet.2007.03.049

Reference yield:

N-(2-chlroethyl)phthalimide (6270-06-0) → 2-(2-azidoethyl)isoindoline-1,3-dione (30250-66-9)

Guidance literature:

With sodium azide; In N,N-dimethyl-formamide;

DOI:10.1016/j.ejmech.2019.111696

upstream raw materials:

2-(2-bromoethyl)isoindoline-1,3-dione

N-(2-Hydroxyethyl)phthalimide

N-(2-chlroethyl)phthalimide

Downstream raw materials:

N-(2-(1,3-dioxoisoindolin-2-yl)ethyl)-2-phenylacetamide

2-[2-(4-phenyl-1H-1,2,3-triazol-1-yl)ethyl]-1H-isoindole-1,3(2H)-dione

N-[2-(2,3-bis(benzyloxy)benzamido)ethyl]phthalimide

C₃₁H₂₅N₅O₃

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