1,3-Di-(3,4,5-trimethoxyphenyl)-1,3-propanedione

Base Information

Chemical Name:1,3-Di-(3,4,5-trimethoxyphenyl)-1,3-propanedione
CAS No.:93199-59-8
Molecular Formula:C₂₁H₂₄O₈
Molecular Weight:404.417
Hs Code.:
Mol file:93199-59-8.mol

Synonyms:

Suppliers and Price of 1,3-Di-(3,4,5-trimethoxyphenyl)-1,3-propanedione

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of 1,3-Di-(3,4,5-trimethoxyphenyl)-1,3-propanedione

Chemical Property:

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

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Useful:

Technology Process of 1,3-Di-(3,4,5-trimethoxyphenyl)-1,3-propanedione

There total 2 articles about 1,3-Di-(3,4,5-trimethoxyphenyl)-1,3-propanedione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 1136-86-3
methyl (3,4,5-trimethoxyphenyl) ketone

: 6178-44-5
ethyl 3,4,5-trimethoxybenzoate

: 93199-59-8
1,3-di-(3,4,5-trimethoxyphenyl)-1,3-propanedione

Guidance literature:: methyl (3,4,5-trimethoxyphenyl) ketone; With sodium hydride; In tetrahydrofuran; at -5 ℃; for 0.5h; Inert atmosphere;

ethyl 3,4,5-trimethoxybenzoate; In tetrahydrofuran; at 20 ℃; for 6h; Inert atmosphere;
DOI:10.1134/S1070363219040315

Reference yield:

: 118-41-2
Eudesmic acid

: 93199-59-8
1,3-di-(3,4,5-trimethoxyphenyl)-1,3-propanedione

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent / conc. H₂SO₄ / 3 h / Heating

2: 38 percent / NaH / benzene / 4 h

With sulfuric acid; sodium hydride; In benzene;
DOI:10.1248/cpb.40.1047

Reference yield: 100.0%

: 1273-86-5
1-ferrocenylmethanol

: 93199-59-8
1,3-di-(3,4,5-trimethoxyphenyl)-1,3-propanedione

: 93122-34-0
C₅H₅FeC₅H₄CH₂CH(COC₆H₂(OCH₃)3)2

Guidance literature:: With HBF₄ or HClO₄; In dichloromethane; byproducts: H2O; aq. HBF4 (45 %) or HClO4 (70 %) added to the Fe-complex and the ketone;soln. stirred (120 min, 20°C), addn. of ether; ethereal soln. washed twice (water), dried (sodium sulfate), solvent removed (vac.), recrystn. (heptane); elem. anal.;