2,6-Bis[(diethylamino)methyl]-4-nitrophenol

Base Information

Chemical Name:2,6-Bis[(diethylamino)methyl]-4-nitrophenol
CAS No.:61150-99-0
Molecular Formula:C16H27N3O3
Molecular Weight:309.409
Hs Code.:
DSSTox Substance ID:DTXSID30558569
Wikidata:Q82440922

Synonyms:61150-99-0;2,6-Bis[(diethylamino)methyl]-4-nitrophenol;DTXSID30558569

Suppliers and Price of 2,6-Bis[(diethylamino)methyl]-4-nitrophenol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2,6-Bis[(diethylamino)methyl]-4-nitrophenol

Chemical Property:

XLogP3:2.5
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:8
Exact Mass:309.20524173
Heavy Atom Count:22
Complexity:303

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CCN(CC)CC1=CC(=CC(=C1O)CN(CC)CC)[N+](=O)[O-]

Technology Process of 2,6-Bis[(diethylamino)methyl]-4-nitrophenol

There total 2 articles about 2,6-Bis[(diethylamino)methyl]-4-nitrophenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 100-02-7,78813-13-5,89830-32-0
4-nitro-phenol

: 109-89-7
diethylamine

: 61150-99-0
2,6-Bis<(diethylamino)methyl>-4-nitrophenol

Guidance literature:: With sodium hydroxide; In ethanol; water; for 60h; Heating;
DOI:10.1016/0022-2860(91)80014-U

Reference yield: 14.99%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 123-30-8
4-amino-phenol

: 109-89-7
diethylamine

: 61150-99-0
2,6-Bis<(diethylamino)methyl>-4-nitrophenol

Guidance literature:: In ethanol; at 80 ℃; for 18h; Sealed tube;

Reference yield:

: 61150-99-0
2,6-Bis<(diethylamino)methyl>-4-nitrophenol

: 4-(7'-bromo-1',5'-naphthyridin-4'-ylamino)-2,6-bis(diethylaminomethyl)phenol

Guidance literature:: Multi-step reaction with 2 steps

1: H₂, NH₃ / Raney nickel / ethanol / 760 Torr / Ambient temperature

2: aq. HCl / methanol / 8 h / 90 - 95 °C

With hydrogenchloride; ammonia; hydrogen; nickel; In methanol; ethanol;