Alanine, 3-[[(phenylmethoxy)carbonyl]amino]-

Base Information

• Chemical Name: Alanine, 3-[[(phenylmethoxy)carbonyl]amino]-
• CAS No.: 61177-01-3
• Molecular Formula: C11H14N2O4
• Molecular Weight: 238.243

Synonyms:(S)-2-Amino-3-benzyloxycarbonylamino-propionic acid;2-Amino-3-benzyloxycarbonylamino-propionsaeure;2-Amino-3-benzyloxycarbonylaminopropionic acid;D-Dap(Z);2-amino-3-benzyloxycarbonylamino-propionic acid;(+-)-2-amino-3-benzyloxycarbonylamino-propionic acid;(+-)-2-Amino-3-benzyloxycarbonylamino-propionsaeure;

Chemical Property of Alanine, 3-[[(phenylmethoxy)carbonyl]amino]-

Chemical Property:

• PSA: 101.65000
• LogP: 1.41590

Purity/Quality:

3-(Cbz-amino)-DL-alanine 97% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Alanine, 3-[[(phenylmethoxy)carbonyl]amino]-

There total 5 articles about Alanine, 3-[[(phenylmethoxy)carbonyl]amino]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.0%

2,3-diaminopropanoic acid (515-94-6) + benzyl chloroformate (501-53-1,94274-21-2) → 2-amino-3-benzyloxycarbonylaminopropionic acid (61177-01-3)

Guidance literature:

2,3-diaminopropanoic acid; benzyl chloroformate; With sodium hydroxide; copper diacetate; magnesium oxide; In water; for 5h; pH=5;

With thioacetamide; acetic acid; In water; for 0.166667h; Heating;

DOI:10.1016/j.bmc.2006.06.023

Reference yield:

diethyl ether (60-29-7,927820-24-4) + 1-methyl-4-nitrosobenzene (623-11-0) + benzyl chloroformate (501-53-1,94274-21-2) + D,L-α,β-diaminopropionic acid monohydrobromide (18635-45-5) → (+/-)-N,N'-dicarbobenzyloxy-2,3-diaminopropanoic acid (42548-08-3) + 2-amino-3-benzyloxycarbonylaminopropionic acid (61177-01-3)

Guidance literature:

Reference yield:

→ 2-amino-3-benzyloxycarbonylaminopropionic acid (61177-01-3)

Guidance literature:

With hydrogenchloride; acetone;

upstream raw materials:

diethyl ether

1-methyl-4-nitrosobenzene

benzyl chloroformate

D,L-α,β-diaminopropionic acid monohydrobromide

Downstream raw materials:

2-amino-3-benzyloxycarbonylamino-propionic acid ethyl ester; hydrochloride

(+/-)-2-benzamino-3-benzyloxycarbonylamino-propionic acid

N²-Acetoacetyl-N³-benzyloxycarbonyl-2,3-diaminopropionsaeure

N³-Benzyloxycarbonyl-2,3-diaminopropionsaeure-tert-butylester

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