2-Phenylbut-2-enedinitrile

Base Information

Chemical Name:2-Phenylbut-2-enedinitrile
CAS No.:61638-11-7
Molecular Formula:C10H6N2
Molecular Weight:154.171
Hs Code.:
DSSTox Substance ID:DTXSID80709105

Synonyms:2-phenylbut-2-enedinitrile;phenyldicyanoethylene;61638-11-7;SCHEMBL3977494;DTXSID80709105

Suppliers and Price of 2-Phenylbut-2-enedinitrile

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of 2-Phenylbut-2-enedinitrile

Chemical Property:

XLogP3:1.6
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:1
Exact Mass:154.053098200
Heavy Atom Count:12
Complexity:265

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)C(=CC#N)C#N

Technology Process of 2-Phenylbut-2-enedinitrile

There total 8 articles about 2-Phenylbut-2-enedinitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.0%

: 27786-05-6
(E)-(1,2-dibromovinyl)benzene

: 544-92-3
copper(I) cyanide

: 61638-11-7
2-phenylfumalonitrile

Guidance literature:: In N,N-dimethyl-formamide; at 130 ℃; for 4h;
DOI:10.1055/s-1991-26544

Reference yield: 9.0%

: 1,3-diphenyltetrazolium tetrafluoroborate

: 764-42-1
1,2-Dicyanoethylene

: 50979-38-9
1,3-diphenyl-1,2,3,4-tetrazolium-5-olate

: 2450-55-7
diphenyl fumarodinitrile

: 6114-57-4
(Z)-2,3-diphenylacrylonitrile

: 61638-11-7
2-phenylfumalonitrile

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; In N,N-dimethyl-formamide; at -60 - 20 ℃; for 3h;
DOI:10.1002/jhet.61

Reference yield:

: 7677-24-9
trimethylsilyl cyanide

: 536-74-3
phenylacetylene

: 61638-11-7
2-phenylfumalonitrile

: 79573-89-0
2-phenylmaleonitrile

Guidance literature:: With oxygen; palladium dichloride; In toluene; at 20 - 100 ℃; under 760.051 Torr; optical yield given as %de; stereoselective reaction;