2-Benzoyl-1-(4-methylphenyl)-4-phenylbutane-1,4-dione

Base Information

Chemical Name:2-Benzoyl-1-(4-methylphenyl)-4-phenylbutane-1,4-dione
CAS No.:61668-29-9
Molecular Formula:C24H20O3
Molecular Weight:356.421
Hs Code.:
DSSTox Substance ID:DTXSID90490153
Nikkaji Number:J3.296.414A

Synonyms:61668-29-9;2-Benzoyl-1-(4-methylphenyl)-4-phenylbutane-1,4-dione;DTXSID90490153

Suppliers and Price of 2-Benzoyl-1-(4-methylphenyl)-4-phenylbutane-1,4-dione

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemicals and raw materials
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Total 0 raw suppliers

Chemical Property of 2-Benzoyl-1-(4-methylphenyl)-4-phenylbutane-1,4-dione

Chemical Property:

XLogP3:4.8
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:7
Exact Mass:356.14124450
Heavy Atom Count:27
Complexity:518

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC=C(C=C1)C(=O)C(CC(=O)C2=CC=CC=C2)C(=O)C3=CC=CC=C3

Technology Process of 2-Benzoyl-1-(4-methylphenyl)-4-phenylbutane-1,4-dione

There total 7 articles about 2-Benzoyl-1-(4-methylphenyl)-4-phenylbutane-1,4-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 19832-78-1
1-(4-methylphenyl)prop-2-en-1-one

: 134-81-6
benzil

: 61668-29-9
2-benzoyl-4-phenyl-1-(p-tolyl)butane-1,4-dione

Guidance literature:: With 3-(2,4,6-trimethyl-phenyl)-5,6,7,8-tetrahydro-4H-cycloheptathiazol-3-ium perchlorate; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 50 ℃; for 12h; Schlenk technique; Inert atmosphere;
DOI:10.1039/c4cc05436a

Reference yield:

: 2431-00-7
p-methylbenzil

: 768-03-6,26742-84-7
Phenyl vinyl ketone

: 61668-26-6
2-benzoyl-1-phenyl-4-(p-tolyl)butane-1,4-dione

: 61668-29-9
2-benzoyl-4-phenyl-1-(p-tolyl)butane-1,4-dione

Guidance literature:: With 3-(2,4,6-trimethyl-phenyl)-5,6,7,8-tetrahydro-4H-cycloheptathiazol-3-ium perchlorate; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 50 ℃; Overall yield = 80 %; Schlenk technique; Inert atmosphere;
DOI:10.1039/c4cc05436a

Reference yield:

: 100-52-7
benzaldehyde

: 61668-29-9
2-benzoyl-4-phenyl-1-(p-tolyl)butane-1,4-dione

Guidance literature:: Multi-step reaction with 3 steps

1: Inert atmosphere; Schlenk technique

2: Inert atmosphere; Schlenk technique

3: N-ethyl-N,N-diisopropylamine; 3-(2,4,6-trimethyl-phenyl)-5,6,7,8-tetrahydro-4H-cycloheptathiazol-3-ium perchlorate / N,N-dimethyl-formamide / 50 °C / Schlenk technique; Inert atmosphere

With 3-(2,4,6-trimethyl-phenyl)-5,6,7,8-tetrahydro-4H-cycloheptathiazol-3-ium perchlorate; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; 3: |Stetter 1,4-Dicarbonyl Synthesis;
DOI:10.1039/c4cc05436a