5-Methoxy-6-[(Z)-1-propenyl]-1,3-benzodioxole

Base Information

Chemical Name:5-Methoxy-6-[(Z)-1-propenyl]-1,3-benzodioxole
CAS No.:23953-63-1
Molecular Formula:C₁₁H₁₂O₃
Molecular Weight:192.214
Hs Code.:
Mol file:23953-63-1.mol

Synonyms:1,3-Benzodioxole,5-methoxy-6-(1-propenyl)-, (Z)-; 1,3-Benzodioxole, 5-methoxy-6-(1Z)-1-propenyl-(9CI); Benzene, 1-methoxy-4,5-(methylenedioxy)-2-propenyl-, (Z)- (8CI);(Z)-Carpacin; Carpacin

Suppliers and Price of 5-Methoxy-6-[(Z)-1-propenyl]-1,3-benzodioxole

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 23 raw suppliers

Chemical Property of 5-Methoxy-6-[(Z)-1-propenyl]-1,3-benzodioxole

Chemical Property:

Vapor Pressure:0.00522mmHg at 25°C
Boiling Point:284.1°Cat760mmHg
Flash Point:94.1°C
PSA：0.00000
Density:1.16g/cm³
LogP:0.00000

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 5-Methoxy-6-[(Z)-1-propenyl]-1,3-benzodioxole

There total 9 articles about 5-Methoxy-6-[(Z)-1-propenyl]-1,3-benzodioxole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 322410-95-7
1,2-methylenedioxy-5-methoxy-4-propynylbenzene

: 23953-63-1
1,2-methylenedioxy-5-methoxy-4-cis-propenylbenzene

Guidance literature:: With hydrogen; Lindlar's catalyst; poisoned with Pb; In quinoline; methanol; under 1551.44 Torr;

Reference yield: 82.0%

: 5780-00-7
2-methoxy-4,5-methylenedioxybenzaldehyde

: 925-90-6
ethylmagnesium bromide

: 194605-01-1,23953-63-1
1,2-methylenedioxy-5-methoxy-4-trans-propenylbenzene

Guidance literature:: 2-methoxy-4,5-methylenedioxybenzaldehyde; ethylmagnesium bromide; In tetrahydrofuran; at 20 ℃; for 1h;

With sulfuric acid; In tetrahydrofuran; for 0.333333h; Heating;

Reference yield:

: 7228-35-5
5-methoxybenzo[d]1,3-dioxole

: 194605-01-1,23953-63-1
1,2-methylenedioxy-5-methoxy-4-trans-propenylbenzene

Guidance literature:: Multi-step reaction with 3 steps

1.1: 92 percent / NBS / CHCl₃

2.1: 90 percent / n-BuLi

3.1: tetrahydrofuran / 1 h / 20 °C

3.2: 82 percent / 5 N aq. H₂SO₄ / tetrahydrofuran / 0.33 h / Heating

With N-Bromosuccinimide; n-butyllithium; In tetrahydrofuran; chloroform;