3,3-Dimethylbicyclo[2.2.1]heptane-2-carbaldehyde

Base Information

• Chemical Name: 3,3-Dimethylbicyclo[2.2.1]heptane-2-carbaldehyde
• CAS No.: 50705-16-3
• Molecular Formula: C10H16 O
• Molecular Weight: 152.236
• European Community (EC) Number: 256-727-0
• DSSTox Substance ID: DTXSID80964954
• Mol file: 50705-16-3.mol

Synonyms:3,3-dimethylbicyclo[2.2.1]heptane-2-carbaldehyde;50705-16-3;EINECS 256-727-0;3,3-Dimethylbicyclo(2.2.1)heptane-2-carbaldehyde;Camphenylal;SCHEMBL11357206;DTXSID80964954;VMKZLKWCFOWLCT-UHFFFAOYSA-N;(1R,4S,5R)-6,6-Dimethylbicyclo[2.2.1]heptane-5-carbaldehyde;Bicyclo(2.2.1)heptane-2-carboxaldehyde, 3,3-dimethyl-

Chemical Property of 3,3-Dimethylbicyclo[2.2.1]heptane-2-carbaldehyde

Chemical Property:

• Vapor Pressure: 0.32mmHg at 25°C
• Boiling Point: 200.7°C at 760 mmHg
• Flash Point: 65.9°C
• PSA: 17.07000
• Density: 1.013g/cm³
• LogP: 2.25760
• XLogP3: 2.6
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 1
• Exact Mass: 152.120115130
• Heavy Atom Count: 11
• Complexity: 183

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC1(C2CCC(C2)C1C=O)C

Technology Process of 3,3-Dimethylbicyclo[2.2.1]heptane-2-carbaldehyde

There total 43 articles about 3,3-Dimethylbicyclo[2.2.1]heptane-2-carbaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

camphene (79-92-5) → 3,3-dimethylbicyclo[2.2.1]heptane-2-carbaldehyde (50705-16-3,361152-33-2,361152-24-1,481660-35-9)

Guidance literature:

With dihydrogen peroxide; methyltrioxorhenium(VII); In chloroform-d1; at 20 ℃; for 3h; Yield given;

Reference yield:

3,3-dimethyl-spiro[norbornan-2,2'-oxirane] (875-03-6,62318-94-9,69685-54-7,69685-55-8,90365-31-4,481660-32-6) → 3,3-dimethylbicyclo[2.2.1]heptane-2-carbaldehyde (50705-16-3,361152-33-2,361152-24-1,481660-35-9)

Guidance literature:

With boron trifluoride diethyl etherate; In benzene; for 8h; Ambient temperature;

Reference yield:

dl-camphene (565-00-4) → 3,3-dimethylbicyclo[2.2.1]heptane-2-carbaldehyde (50705-16-3,361152-33-2,361152-24-1,481660-35-9)

Guidance literature:

With chromyl chloride; camphenilanaldehyde; Behandeln des Reaktionsprodukts mit Wasser;

upstream raw materials:

2,2,3-trimethyl-bicyclo[2.2.1]heptane

2.2-Dimethyl-3-oxymethyl-bicyclo-[1.2.2]-heptan

2-endo-hydroxymethyl-3,3-dimethylbicyclo[2.2.1]heptane-2-exo-ol

dl-camphene

Downstream raw materials:

2.2-Dimethyl-3-oxymethyl-bicyclo-[1.2.2]-heptan

3,3-dimethylbicyclo[2.2.1]heptane-2-carbaldehyde

5,5-Dimethyl-1,3-dioxocyclohex-2-yl-5',5'-dimethyl-1'-oxo-3'-hydroxy-cyclohex-2'-en-2'-yl-3'',3''-dimethylbicyclo<2.2.1>hept-2''-exo-yl-methan

(E)-3-((1S,2S,4R)-3,3-Dimethyl-bicyclo[2.2.1]hept-2-yl)-acrylic acid

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