1,1'-(1,2,2-Trimethoxyethane-1,1-diyl)dibenzene

Base Information

• Chemical Name: 1,1'-(1,2,2-Trimethoxyethane-1,1-diyl)dibenzene
• CAS No.: 62134-83-2
• Molecular Formula: C₁₇H₂₀O₃
• Molecular Weight: 272.344
• DSSTox Substance ID: DTXSID10555354
• Wikidata: Q82436677

Synonyms:62134-83-2;1,1'-(1,2,2-Trimethoxyethane-1,1-diyl)dibenzene;DTXSID10555354

Chemical Property of 1,1'-(1,2,2-Trimethoxyethane-1,1-diyl)dibenzene

Chemical Property:

• XLogP3: 3
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 6
• Exact Mass: 272.14124450
• Heavy Atom Count: 20
• Complexity: 245

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: COC(C(C1=CC=CC=C1)(C2=CC=CC=C2)OC)OC

Technology Process of 1,1'-(1,2,2-Trimethoxyethane-1,1-diyl)dibenzene

There total 4 articles about 1,1'-(1,2,2-Trimethoxyethane-1,1-diyl)dibenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 38.0%

methanol (67-56-1) + Phenylselenyl chloride (5707-04-0) + cis-stilben (645-49-8) → 1,2-diphenyl-1,2-dimethoxy ethane, meso (3962-43-4) + 1,1-diphenyl-1,2,2-trimethoxy ethane (62134-83-2) + (+/-)-1,2-dimethoxy-1,2-diphenylethane (1147-17-7,3962-43-4,14156-28-6,40577-73-9,62860-42-8,62860-43-9) + 1,2-diphenyl-1-methoxy-2-chloro ethane, threo (116118-05-9,116118-06-0,133810-05-6,133810-06-7)

Guidance literature:

for 5h; Heating;

DOI:10.1016/S0040-4020(01)81734-8

Reference yield: 38.0%

methanol (67-56-1) + Phenylselenyl chloride (5707-04-0) + (E)-1,2-diphenyl-ethene (103-30-0) → 1,2-diphenyl-1,2-dimethoxy ethane, meso (3962-43-4) + 1,1-diphenyl-1,2,2-trimethoxy ethane (62134-83-2) + (+/-)-1,2-dimethoxy-1,2-diphenylethane (1147-17-7,3962-43-4,14156-28-6,40577-73-9,62860-42-8,62860-43-9) + 1,2-diphenyl-1-methoxy-2-chloro ethane, erythro (116118-05-9,116118-06-0,133810-05-6,133810-06-7)

Guidance literature:

for 5h; Heating;

DOI:10.1016/S0040-4020(01)81734-8

Reference yield:

Diphenylacetaldehyde (947-91-1) → 1,1-diphenyl-1,2,2-trimethoxy ethane (62134-83-2)

Guidance literature:

Multi-step reaction with 2 steps

1: (i), (ii) N-chloro-succinimide, CCl₄

DOI:10.1016/0040-4020(76)87034-2

upstream raw materials:

methanol

N-1-(2-Chlor-2,2-diphenylethyliden)-tert-butylamin

Phenylselenyl chloride

cis-stilben

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