1-methoxy-N,N-dimethylmethanamine

Base Information

• Chemical Name: 1-methoxy-N,N-dimethylmethanamine
• CAS No.: 62393-45-7
• Molecular Formula: C4H11NO
• Molecular Weight: 89.1374
• European Community (EC) Number: 823-795-3
• DSSTox Substance ID: DTXSID60574813
• Nikkaji Number: J952.625K
• Wikidata: Q82463982
• Mol file: 62393-45-7.mol

Synonyms:62393-45-7;1-methoxy-N,N-dimethylmethanamine;(methoxymethyl)dimethylamine;(DIMETHYLAMINO)METHYL METHYL ETHER;methoxymethyldimethylamine;DTXSID60574813;(DIMETHYLAMINO)METHYLMETHYLETHER;EN300-1720855

Chemical Property of 1-methoxy-N,N-dimethylmethanamine

Chemical Property:

• PSA: 12.47000
• LogP: 0.15190
• XLogP3: 0.2
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 2
• Exact Mass: 89.084063974
• Heavy Atom Count: 6
• Complexity: 28.7

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CN(C)COC

Technology Process of 1-methoxy-N,N-dimethylmethanamine

There total 5 articles about 1-methoxy-N,N-dimethylmethanamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

dimethylsulfite (616-42-2) + (dimethylamino)methyl acetate (2036-94-4) → acetic acid methyl ester (79-20-9) + dimethylaminomethylsulfonic acid (68507-34-6) + methoxy bis(dimethylamino)methane (62393-45-7) + (trimethylammonio)methanesulfonate

Guidance literature:

With dimethylsulfite; at 25 ℃; for 336h;

DOI:10.1007/BF00952877

Reference yield: 64.0%

dimethylsulfite (616-42-2) + N-(chloromethyl)dimethylamine (30438-74-5) → methylene chloride (74-87-3) + dimethylaminomethylsulfonic acid (68507-34-6) + methoxy bis(dimethylamino)methane (62393-45-7) + (trimethylammonio)methanesulfonate

Guidance literature:

at 80 ℃; for 5h; Product distribution; other temperatures, time; reaction of dimethyl sulfite with dimethylammonium derivatives Me₂NCH₂X (X = Cl, CF₃CO₂, CCl₃CO₂, MeCO₂);

DOI:10.1007/BF00952877

Reference yield:

dimethylsulfite (616-42-2) + Trichloro-acetic acid dimethylaminomethyl ester → dimethylaminomethylsulfonic acid (68507-34-6) + Methyl trichloroacetate (598-99-2) + methoxy bis(dimethylamino)methane (62393-45-7) + (trimethylammonio)methanesulfonate

Guidance literature:

at 50 ℃; for 5h; Yields of byproduct given;

DOI:10.1007/BF00952877

upstream raw materials:

dimethylsulfite

(dimethylamino)methyl acetate

N-(chloromethyl)dimethylamine

Downstream raw materials:

N,N-Dimethylamino acetonitrile

C₂₂H₂₇NO₂

2-(4-benzyloxy-phenyl)-1-cyclohexyl-3-dimethylamino-propenone

1-cyclohexyl-3-dimethylamino-2-(4-iodo-phenyl)-propenone

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