(Dimethylamino)methyl Methyl Ether

Base Information

• Chemical Name: (Dimethylamino)methyl Methyl Ether
• CAS No.: 62393-45-7
• Molecular Formula: C4H11NO
• Molecular Weight: 89.1374
• Mol file: 62393-45-7.mol

Synonyms:N-methoxymethyl-N,N-dimethylamine;methylmethyldimethylamine;Methanamine,1-methoxy-N,N-dimethyl;

Chemical Property of (Dimethylamino)methyl Methyl Ether

Chemical Property:

• PSA: 12.47000
• LogP: 0.15190

Purity/Quality:

99%min ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of (Dimethylamino)methyl Methyl Ether

There total 5 articles about (Dimethylamino)methyl Methyl Ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

dimethylsulfite (616-42-2) + (dimethylamino)methyl acetate (2036-94-4) → acetic acid methyl ester (79-20-9) + dimethylaminomethylsulfonic acid (68507-34-6) + methoxy bis(dimethylamino)methane (62393-45-7) + (trimethylammonio)methanesulfonate

Guidance literature:

With dimethylsulfite; at 25 ℃; for 336h;

DOI:10.1007/BF00952877

Reference yield: 64.0%

dimethylsulfite (616-42-2) + N-(chloromethyl)dimethylamine (30438-74-5) → methylene chloride (74-87-3) + dimethylaminomethylsulfonic acid (68507-34-6) + methoxy bis(dimethylamino)methane (62393-45-7) + (trimethylammonio)methanesulfonate

Guidance literature:

at 80 ℃; for 5h; Product distribution; other temperatures, time; reaction of dimethyl sulfite with dimethylammonium derivatives Me₂NCH₂X (X = Cl, CF₃CO₂, CCl₃CO₂, MeCO₂);

DOI:10.1007/BF00952877

Reference yield:

dimethylsulfite (616-42-2) + Trichloro-acetic acid dimethylaminomethyl ester → dimethylaminomethylsulfonic acid (68507-34-6) + Methyl trichloroacetate (598-99-2) + methoxy bis(dimethylamino)methane (62393-45-7) + (trimethylammonio)methanesulfonate

Guidance literature:

at 50 ℃; for 5h; Yields of byproduct given;

DOI:10.1007/BF00952877

upstream raw materials:

dimethylsulfite

(dimethylamino)methyl acetate

N-(chloromethyl)dimethylamine

Downstream raw materials:

N,N-Dimethylamino acetonitrile

C₂₃H₂₇NO₂S

1-cyclohexyl-3-dimethylamino-2-(4-iodo-phenyl)-propenone

2-(4-benzyloxy-phenyl)-1-cyclohexyl-3-dimethylamino-propenone

Refernces