dimethylaminomethylsulfonic acid

Base Information

• Chemical Name: dimethylaminomethylsulfonic acid
• CAS No.: 68507-34-6
• Molecular Formula: C₃H₉NO₃S
• Molecular Weight: 139.175

Synonyms:dimethylaminomethylsulfonic acid

Chemical Property of dimethylaminomethylsulfonic acid

Chemical Property:

• Density: 1.340±0.06 g/cm3(Predicted)

Purity/Quality:

99.0%min ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
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Technology Process of dimethylaminomethylsulfonic acid

There total 5 articles about dimethylaminomethylsulfonic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

dimethylsulfite (616-42-2) + (dimethylamino)methyl acetate (2036-94-4) → acetic acid methyl ester (79-20-9) + dimethylaminomethylsulfonic acid (68507-34-6) + methoxy bis(dimethylamino)methane (62393-45-7) + (trimethylammonio)methanesulfonate

Guidance literature:

With dimethylsulfite; at 25 ℃; for 336h;

DOI:10.1007/BF00952877

Reference yield: 64.0%

dimethylsulfite (616-42-2) + N-(chloromethyl)dimethylamine (30438-74-5) → methylene chloride (74-87-3) + dimethylaminomethylsulfonic acid (68507-34-6) + methoxy bis(dimethylamino)methane (62393-45-7) + (trimethylammonio)methanesulfonate

Guidance literature:

at 80 ℃; for 5h; Product distribution; other temperatures, time; reaction of dimethyl sulfite with dimethylammonium derivatives Me₂NCH₂X (X = Cl, CF₃CO₂, CCl₃CO₂, MeCO₂);

DOI:10.1007/BF00952877

Reference yield:

dimethylsulfite (616-42-2) + Trichloro-acetic acid dimethylaminomethyl ester → dimethylaminomethylsulfonic acid (68507-34-6) + Methyl trichloroacetate (598-99-2) + methoxy bis(dimethylamino)methane (62393-45-7) + (trimethylammonio)methanesulfonate

Guidance literature:

at 50 ℃; for 5h; Yields of byproduct given;

DOI:10.1007/BF00952877

upstream raw materials:

dimethylsulfite

(dimethylamino)methyl acetate

N-(chloromethyl)dimethylamine

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