9-(3-Methylphenyl)-9H-fluorene

Base Information

Chemical Name:9-(3-Methylphenyl)-9H-fluorene
CAS No.:18153-42-9
Molecular Formula:C20H16
Molecular Weight:256.341
Hs Code.:
DSSTox Substance ID:DTXSID40171162
Nikkaji Number:J1.557.281G
Wikidata:Q83041254
Mol file:18153-42-9.mol

Synonyms:9-(3-METHYLPHENYL)-9H-FLUORENE;18153-42-9;9-m-tolylfluorene;DTXSID40171162

Suppliers and Price of 9-(3-Methylphenyl)-9H-fluorene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of 9-(3-Methylphenyl)-9H-fluorene

Chemical Property:

Vapor Pressure:4.85E-06mmHg at 25°C
Boiling Point:393.4°Cat760mmHg
Flash Point:185.5°C
Density:1.12g/cm³
XLogP3:5.4
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:1
Exact Mass:256.125200510
Heavy Atom Count:20
Complexity:311

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC(=CC=C1)C2C3=CC=CC=C3C4=CC=CC=C24

Technology Process of 9-(3-Methylphenyl)-9H-fluorene

There total 9 articles about 9-(3-Methylphenyl)-9H-fluorene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 86-73-7
9H-fluorene

: 108-41-8
1-chloro-3-methylbenzene

: 18153-42-9
9-(3-methylphenyl)-9H-fluorene

Guidance literature:: With NHC-Pd(II)-Im; potassium tert-butylate; In 1,4-dioxane; at 120 ℃; for 12h; Inert atmosphere; Schlenk technique;
DOI:10.1039/c4ob01594k

Reference yield: 92.0%

: 2947-60-6
3-methylbenzyl cyanide

: 1016-05-3
dibenzothiophene sulfone

: 18153-42-9
9-(3-methylphenyl)-9H-fluorene

Guidance literature:: With potassium hexamethylsilazane; In toluene; Petroleum ether; at 100 ℃; for 24h; Inert atmosphere;
DOI:10.1039/c8ob02355g

Reference yield:

: 352-32-9
p-fluorotoluene

: 86-73-7
9H-fluorene

: 18153-42-9
9-(3-methylphenyl)-9H-fluorene

: 18153-43-0
9-(4-methylphenyl)fluorene

Guidance literature:: 9H-fluorene; With lithium diisopropyl amide; In tetrahydrofuran; at 25 ℃; Inert atmosphere;

p-fluorotoluene; In tetrahydrofuran; at 25 ℃; Overall yield = 83 %; Overall yield = 225.8 mg; Inert atmosphere;
DOI:10.1021/acs.orglett.5b02602