Pyridine, 4-[(phenylsulfonyl)methyl]-, 1-oxide

Base Information

Chemical Name:Pyridine, 4-[(phenylsulfonyl)methyl]-, 1-oxide
CAS No.:62586-62-3
Molecular Formula:C12H11NO3S
Molecular Weight:249.29
Hs Code.:
DSSTox Substance ID:DTXSID40458788
Wikidata:Q82282310

Synonyms:62586-62-3;Pyridine, 4-[(phenylsulfonyl)methyl]-, 1-oxide;DTXSID40458788

Suppliers and Price of Pyridine, 4-[(phenylsulfonyl)methyl]-, 1-oxide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Pyridine, 4-[(phenylsulfonyl)methyl]-, 1-oxide

Chemical Property:

XLogP3:0
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:3
Exact Mass:249.04596439
Heavy Atom Count:17
Complexity:322

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)S(=O)(=O)CC2=CC=[N+](C=C2)[O-]

Technology Process of Pyridine, 4-[(phenylsulfonyl)methyl]-, 1-oxide

There total 2 articles about Pyridine, 4-[(phenylsulfonyl)methyl]-, 1-oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 1620-52-6
4-((benzenesulfonyl)methyl)pyridine

: 62586-62-3
4-(benzenesulfonylmethyl)pyridine N-oxide

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 0 - 20 ℃; for 12h;
DOI:10.1055/s-2004-822311

Reference yield:

: 873-55-2
sodium benzenesulfonate

: 62586-62-3
4-(benzenesulfonylmethyl)pyridine N-oxide

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent / tetrapropylammonium bromide; DBU / acetonitrile / 24 h / 80 °C

2: 93 percent / MCPBA / CH₂Cl₂ / 12 h / 0 - 20 °C

With tetra-n-propylammonium bromide; 1,8-diazabicyclo[5.4.0]undec-7-ene; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; acetonitrile;
DOI:10.1055/s-2004-822311

Reference yield: 74.0%

: 62586-62-3
4-(benzenesulfonylmethyl)pyridine N-oxide

: 100-39-0
benzyl bromide

: 866392-97-4
benzyl dithioisonicotinate N-oxide

Guidance literature:: 4-(benzenesulfonylmethyl)pyridine N-oxide; With potassium tert-butylate; sulfur; In tetrahydrofuran;

benzyl bromide; In tetrahydrofuran; Further stages.;
DOI:10.1021/ma050652d