1-Methoxy-1-(trichloromethyl)cyclohexane

Base Information

Chemical Name:1-Methoxy-1-(trichloromethyl)cyclohexane
CAS No.:62688-90-8
Molecular Formula:C8H13Cl3O
Molecular Weight:231.54700
Hs Code.:
DSSTox Substance ID:DTXSID30559834
Wikidata:Q82442687

Synonyms:1-Methoxy-1-(trichloromethyl)cyclohexane;62688-90-8;DTXSID30559834

Suppliers and Price of 1-Methoxy-1-(trichloromethyl)cyclohexane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 1-Methoxy-1-(trichloromethyl)cyclohexane

Chemical Property:

Boiling Point:120-121 °C(Press: 15 Torr)
PSA：9.23000
Density:1.2763 g/cm3
LogP:3.70590
XLogP3:3.6
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:1
Exact Mass:230.003198
Heavy Atom Count:12
Complexity:147

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1(CCCCC1)C(Cl)(Cl)Cl

Technology Process of 1-Methoxy-1-(trichloromethyl)cyclohexane

There total 4 articles about 1-Methoxy-1-(trichloromethyl)cyclohexane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

: 3508-84-7
1-(trichloromethyl)cyclohexan-1-ol

: 77-78-1
dimethyl sulfate

: 62688-90-8
1-Methoxy-1-trichlormethyl-cyclohexan

Guidance literature:: With sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride; In chloroform; at 95 - 100 ℃; for 0.5h;

Reference yield:

: 3508-84-7
1-(trichloromethyl)cyclohexan-1-ol

: 74-88-4
methyl iodide

: 62688-90-8
1-Methoxy-1-trichlormethyl-cyclohexan

Guidance literature:: With sodium hydroxide; tetra-(n-butyl)ammonium iodide; In benzene; at 30 - 35 ℃; for 1h; Yield given;

Reference yield:

: 108-94-1,11119-77-0,9003-41-2,9075-99-4
cyclohexanone

: 62688-90-8
1-Methoxy-1-trichlormethyl-cyclohexan

Guidance literature:: Multi-step reaction with 2 steps

1: 36 percent / liq. NH₃, t-BuOK / 0.5 h / -75 - -65 °C

2: 48 percent / benzyltriethylammonium chloride, 50percent aq. sodium hydroxide / CHCl₃ / 0.5 h / 95 - 100 °C

With sodium hydroxide; potassium tert-butylate; N-benzyl-N,N,N-triethylammonium chloride; ammonia; In chloroform;