4-BroMo-N-(4-chlorophenyl)benzenesulfonaMide, 97%

Base Information

• Chemical Name: 4-BroMo-N-(4-chlorophenyl)benzenesulfonaMide, 97%
• CAS No.: 6295-97-2
• Molecular Formula: C12H9BrClNO2S
• Molecular Weight: 346.632
• Mol file: 6295-97-2.mol

Synonyms:4-Brom-benzolsulfonsaeure-(4-chlor-anilid);4-Bromo-N-(4-chloro-phenyl)-benzenesulfonamide;

Chemical Property of 4-BroMo-N-(4-chlorophenyl)benzenesulfonaMide, 97%

Chemical Property:

• Melting Point: 135.5 °C (ethanol)
• PSA: 54.55000
• LogP: 5.05710

Purity/Quality:

99% ^*data from raw suppliers

4-Bromo-N-(4-chloro-phenyl)-benzenesulfonamide 95 ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 4-BroMo-N-(4-chlorophenyl)benzenesulfonaMide, 97%

There total 12 articles about 4-BroMo-N-(4-chlorophenyl)benzenesulfonaMide, 97% which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

4-bromo-N-(4-chlorophenyl)-N-cyanobenzenesulfonamide + 4-pyridylboronic acid (1692-15-5) → pyridine-4-carbonitrile (100-48-1) + 4-bromo-benzenesulfonic acid-(4-chloro-anilide) (6295-97-2)

Guidance literature:

With Fe3O4/SiO2/(3-chloropropyl)trimethoxysilane/2,2′-(4,4′-(propane-1,3-diyl)bis(piperazine-4,1-diyl))- diethanamine/Pd; In acetonitrile; for 10h; Catalytic behavior; Reflux;

DOI:10.1016/j.ica.2020.119956

Reference yield: 93.0%

4-bromo-N-(4-chlorophenyl)-N-cyanobenzenesulfonamide + 1,3-phenylenediboronic acid (4612-28-6) → benzene-1,3-dicarbonitrile (626-17-5) + 4-bromo-benzenesulfonic acid-(4-chloro-anilide) (6295-97-2)

Guidance literature:

With Fe3O4/SiO2/(3-chloropropyl)trimethoxysilane/2,2′-(4,4′-(propane-1,3-diyl)bis(piperazine-4,1-diyl))- diethanamine/Pd; In acetonitrile; for 15h; Catalytic behavior; Reflux;

DOI:10.1016/j.ica.2020.119956

Reference yield: 92.0%

4-Chlorophenylboronic acid (1679-18-1) + 4-bromo-N-(4-chlorophenyl)-N-cyanobenzenesulfonamide → 4-Cyanochlorobenzene (623-03-0) + 4-bromo-benzenesulfonic acid-(4-chloro-anilide) (6295-97-2)

Guidance literature:

With Fe3O4/SiO2/(3-chloropropyl)trimethoxysilane/2,2′-(4,4′-(propane-1,3-diyl)bis(piperazine-4,1-diyl))- diethanamine/Pd; In acetonitrile; for 13h; Catalytic behavior; Reflux;

DOI:10.1016/j.ica.2020.119956

upstream raw materials:

4-chloro-aniline

4-bromobenzenesulfonyl chloride

3-chlorophenylboronic acid

4-Chlorophenylboronic acid

Downstream raw materials:

4-bromo-benzenesulfonic acid-(N-ethyl-4-chloro-anilide)

4-bromo-benzenesulfonic acid-[4-chloro-N-(2-chloro-ethyl)-anilide]

4-bromo-benzenesulfonic acid-(4-chloro-N-methyl-anilide)