1,2-Benzisothiazol-3(2H)-one, 2-(4-methylphenyl)-, 1,1-dioxide

Base Information

Chemical Name:1,2-Benzisothiazol-3(2H)-one, 2-(4-methylphenyl)-, 1,1-dioxide
CAS No.:63113-47-3
Molecular Formula:C14H11NO3S
Molecular Weight:273.312
Hs Code.:
DSSTox Substance ID:DTXSID90450590
Nikkaji Number:J767.801K
Wikidata:Q82270377

Synonyms:63113-47-3;1,2-Benzisothiazol-3(2H)-one, 2-(4-methylphenyl)-, 1,1-dioxide;DTXSID90450590;2-p-Tolyl-1,2-benzisothiazole-3(2H)-one 1,1-dioxide

Suppliers and Price of 1,2-Benzisothiazol-3(2H)-one, 2-(4-methylphenyl)-, 1,1-dioxide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 1,2-Benzisothiazol-3(2H)-one, 2-(4-methylphenyl)-, 1,1-dioxide

Chemical Property:

XLogP3:2.5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:1
Exact Mass:273.04596439
Heavy Atom Count:19
Complexity:460

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC=C(C=C1)N2C(=O)C3=CC=CC=C3S2(=O)=O

Technology Process of 1,2-Benzisothiazol-3(2H)-one, 2-(4-methylphenyl)-, 1,1-dioxide

There total 12 articles about 1,2-Benzisothiazol-3(2H)-one, 2-(4-methylphenyl)-, 1,1-dioxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 3076-56-0
p-tolyllead triacetate

: 128-44-9
saccharin sodium salt

: 63113-47-3
2-(p-tolyl)benzo[d]isothiazol-3(2H)-one-1,1-dioxide

Guidance literature:: With copper diacetate; In dichloromethane; N,N-dimethyl-formamide; at 60 ℃; for 5h;
DOI:10.1016/S0040-4039(00)61799-9

Reference yield: 92.0%

: 5720-05-8
4-methylphenylboronic acid

: 81-07-2
saccharin

: 63113-47-3
2-(p-tolyl)benzo[d]isothiazol-3(2H)-one-1,1-dioxide

Guidance literature:: With pyridine; copper diacetate; In dichloromethane; for 53h; Ambient temperature;
DOI:10.1016/S0040-4039(98)00503-6

Reference yield: 86.0%

: C₁₃H₁₂INO₂S

: 1864-94-4
phenyl formate

: 63113-47-3
2-(p-tolyl)benzo[d]isothiazol-3(2H)-one-1,1-dioxide

Guidance literature:: With palladium diacetate; triethylamine; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; In toluene; at 80 ℃; for 18h; Schlenk technique; Inert atmosphere;
DOI:10.1055/s-0036-1588422