2-Methoxy-5-phenyloxolane

Base Information

Chemical Name:2-Methoxy-5-phenyloxolane
CAS No.:63298-04-4
Molecular Formula:C11H14O2
Molecular Weight:178.22800
Hs Code.:
DSSTox Substance ID:DTXSID30496199

Synonyms:63298-04-4;2-methoxy-5-phenyltetrahydrofuran;2-Methoxy-5-phenyloxolane;DTXSID30496199

Suppliers and Price of 2-Methoxy-5-phenyloxolane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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Total 0 raw suppliers

Chemical Property of 2-Methoxy-5-phenyloxolane

Chemical Property:

Boiling Point:266.7±40.0 °C(Predicted)
PSA：18.46000
Density:1.06±0.1 g/cm3(Predicted)
LogP:2.51060
XLogP3:2.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:178.099379685
Heavy Atom Count:13
Complexity:152

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1CCC(O1)C2=CC=CC=C2

Technology Process of 2-Methoxy-5-phenyloxolane

There total 8 articles about 2-Methoxy-5-phenyloxolane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 67-56-1
methanol

: 53634-77-8
4-(Methylthio)-1-phenyl-3-buten-1-ol

: 63298-04-4
tetrahydro-2-methoxy-5-phenylfuran

Guidance literature:: With mercury dichloride; for 20h; Ambient temperature;

Reference yield:

: 696-59-3
cis,trans-2,5-dimethoxytetrahydrofuran

: 63298-04-4
tetrahydro-2-methoxy-5-phenylfuran

Guidance literature:: Multi-step reaction with 2 steps

1: 58 percent / CaCl₂ / CH₂Cl₂ / 24 h / Ambient temperature

2: 1.) Mg, ZnBr₂, / 1.) THF, RT; 30 min, 2.) THF, RT;

With magnesium; calcium chloride; zinc dibromide; In dichloromethane;
DOI:10.1016/S0040-4020(01)81323-5