Phenol, 2-[[(3-hydroxypropyl)imino]phenylmethyl]-

Base Information

Chemical Name:Phenol, 2-[[(3-hydroxypropyl)imino]phenylmethyl]-
CAS No.:63329-82-8
Molecular Formula:C₁₆H₁₇NO₂
Molecular Weight:255.316
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Phenol, 2-[[(3-hydroxypropyl)imino]phenylmethyl]-

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Phenol, 2-[[(3-hydroxypropyl)imino]phenylmethyl]-

There total 2 articles about Phenol, 2-[[(3-hydroxypropyl)imino]phenylmethyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 117-99-7
2-Hydroxybenzophenone

: 156-87-6
propan-1-ol-3-amine

: 63329-82-8
(E)-2-(((3-hydroxypropyl)imino)(phenyl)methyl)phenol

Guidance literature:: With magnesium sulfate; In ethanol; Reflux;
DOI:10.1021/jacs.5b00822

Reference yield:

: 63329-82-8
(E)-2-(((3-hydroxypropyl)imino)(phenyl)methyl)phenol

Guidance literature:: 2-Hydroxy-benzophenon, entspr. Amin;

Reference yield:

: 63329-82-8
HOC₆H₄C(C₆H₅)N(CH₂)3OH

: 4612-26-4
1,4-Phenyldiboronic acid

: 855308-50-8
C₆H₄(B(OC₆H₄C(C₆H₅)N(CH₂)3O))2

Guidance literature:: In tetrahydrofuran; byproducts: H2O; mixt. of ligand and B compd. (molar ratio 2:1) in THF refluxed for 1 h under stirring; H2O and solvent removed partially with Dean-Stark trap; filtered; ppt. washed with hexane; detd. by mass spectrometry;
DOI:10.1016/j.jorganchem.2005.01.060