(5Z)-5-[3-bromo-4-(dimethylamino)benzylidene]-1-methylpyrimidine-2,4,6(1H,3H,5H)-trione

Base Information

• Chemical Name: (5Z)-5-[3-bromo-4-(dimethylamino)benzylidene]-1-methylpyrimidine-2,4,6(1H,3H,5H)-trione
• CAS No.: 5960-64-5
• Molecular Formula: C21H15 N O2
• Molecular Weight: 313.356

Synonyms:Anthraquinone, 1-(benzylamino)-(7CI,8CI); 1-(Benzylamino)anthraquinone

Chemical Property of (5Z)-5-[3-bromo-4-(dimethylamino)benzylidene]-1-methylpyrimidine-2,4,6(1H,3H,5H)-trione

Chemical Property:

• Boiling Point: °Cat760mmHg
• Flash Point: °C
• Density: 1.565g/cm³

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of (5Z)-5-[3-bromo-4-(dimethylamino)benzylidene]-1-methylpyrimidine-2,4,6(1H,3H,5H)-trione

There total 7 articles about (5Z)-5-[3-bromo-4-(dimethylamino)benzylidene]-1-methylpyrimidine-2,4,6(1H,3H,5H)-trione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

1-amino-9,10-anthracenedione (82-45-1) + benzyl chloride (100-44-7) → 1-(benzylamino)-9,10-anthraquinone (5960-64-5)

Guidance literature:

With potassium hydroxide; In dimethyl sulfoxide; at 30 ℃;

DOI:10.1246/cl.1981.1789

Reference yield: 90.0%

1-chloroanthracene-9,10-dione (82-44-0) + benzylamine (100-46-9) → 1-(benzylamino)-9,10-anthraquinone (5960-64-5)

Guidance literature:

at 160 ℃; for 6h; Sealed tube;

DOI:10.1021/acschemneuro.0c00624

Reference yield: 40.0%

1-amino-9,10-anthracenedione (82-45-1) + benzaldehyde (100-52-7) → 1-(benzylamino)-9,10-anthraquinone (5960-64-5)

Guidance literature:

With zinc(II) chloride; for 10h; Heating;

upstream raw materials:

pyridine

1-nitroanthraquinone

benzylamine

1-amino-9,10-anthracenedione

Downstream raw materials:

1-amino-9,10-anthracenedione

1-benzylidene-2-(2,4-dinitrophenyl)hydrazone

spiro<1-dibenzylamino-10-anthrone-9,3'-<2>phenyloxirane>

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