Trimethyl 4,5,6-trichlorobenzene-1,2,3-tricarboxylate

Base Information

Chemical Name:Trimethyl 4,5,6-trichlorobenzene-1,2,3-tricarboxylate
CAS No.:6421-52-9
Molecular Formula:C₁₂H₉Cl₃O₆
Molecular Weight:355.559
Hs Code.:
DSSTox Substance ID:DTXSID20576151
Wikidata:Q82465701

Synonyms:6421-52-9;Trimethyl 4,5,6-trichlorobenzene-1,2,3-tricarboxylate;DTXSID20576151

Suppliers and Price of Trimethyl 4,5,6-trichlorobenzene-1,2,3-tricarboxylate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of Trimethyl 4,5,6-trichlorobenzene-1,2,3-tricarboxylate

Chemical Property:

XLogP3:3.6
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:6
Rotatable Bond Count:6
Exact Mass:353.946471
Heavy Atom Count:21
Complexity:399

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC(=O)C1=C(C(=C(C(=C1C(=O)OC)Cl)Cl)Cl)C(=O)OC

Technology Process of Trimethyl 4,5,6-trichlorobenzene-1,2,3-tricarboxylate

There total 4 articles about Trimethyl 4,5,6-trichlorobenzene-1,2,3-tricarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 67-56-1
methanol

: 102325-38-2
1,7,8,9-Tetrachloro-10,10-dimethoxy-4-oxa-tricyclo[5.2.1.0^2,6]deca-2⁽⁶⁾,8-diene-3,5-dione

: 6421-52-9
trimethyl 4,5,6-trichlorophenyltricarboxylate

Guidance literature:: With toluene-4-sulfonic acid; at 60 ℃;
DOI:10.1039/c39850001589

Reference yield:

: 2207-27-4
5,5-dimethoxy-1,2,3,4-tetrachlorocyclopentadiene

: 6421-52-9
trimethyl 4,5,6-trichlorophenyltricarboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) 160 deg C, 10 h, 2.) room temperature, 16 h; reflux, 10 min

2: 70 g / Zn, AcOH / 18 h

3: 10 percent / p-TsOH / 3 h / Heating

With toluene-4-sulfonic acid; acetic acid; zinc;
DOI:10.1039/P19940000721

Reference yield:

: (1R,2R,3S,6S,7S)-2,3-Dibromo-1,7,8,9-tetrachloro-6-methoxy-4-oxo-5-oxa-tricyclo[4.3.0.0^3,7]non-8-ene-2-carboxylic acid methyl ester

: 6421-52-9
trimethyl 4,5,6-trichlorophenyltricarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: 70 g / Zn, AcOH / 18 h

2: 10 percent / p-TsOH / 3 h / Heating

With toluene-4-sulfonic acid; acetic acid; zinc;
DOI:10.1039/P19940000721