1,3-Dimethyl-5,5-diphenylimidazolidine-2,4-dione

Base Information

• Chemical Name: 1,3-Dimethyl-5,5-diphenylimidazolidine-2,4-dione
• CAS No.: 6456-01-5
• Molecular Formula: C17H16N2O2
• Molecular Weight: 280.326
• Mol file: 6456-01-5.mol

Synonyms:2,4-Imidazolidinedione,1,3-dimethyl-5,5-diphenyl;2,4-Imidazolidinedione, 1,3-dimethyl-5,5-diphenyl-;1,3-Dimethyl-5,5-diphenyl-imidazolidin-2,4-dion;1,3-dimethyl-5,5-diphenyl-imidazolidine-2,4-dione;1,3-dimethyl-5,5-diphenyl-tetrahydro-imidazole-2,4-dione;1,3-Dimethyl-5,5-diphenyl-hydantoin;1,3-dimethylphenytoin;

Chemical Property of 1,3-Dimethyl-5,5-diphenylimidazolidine-2,4-dione

Chemical Property:

• PSA: 40.62000
• LogP: 2.32980

Purity/Quality:

95% ^*data from raw suppliers

1,3-DIMETHYL-5,5-DIPHENYL-2,4-IMIDAZOLIDINEDIONE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1,3-Dimethyl-5,5-diphenylimidazolidine-2,4-dione

There total 11 articles about 1,3-Dimethyl-5,5-diphenylimidazolidine-2,4-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

N,N'-Dimethylurea (96-31-1) + benzil (134-81-6) → 1,3-dimethyl-5,5-diphenylhydantoin (6456-01-5)

Guidance literature:

With polymer supported zinc(II)-salen complex; In ethanol; water; at 65 ℃; for 4h; Green chemistry;

DOI:10.1007/s11164-017-3215-x

Reference yield: 83.0%

1,3-dimethyl-4,5-diphenyl-4,5-dihydroxyimidazolidin-2-one (66242-64-6) + 1-<2-(N,N-Dimethylamino)ethyl>urea hydrochloride → 6-[2-(dimethylamino)ethyl]-2,4-dimethyl-1,5-diphenylglycoluril hydrochloride + 1,3-dimethyl-5,5-diphenylhydantoin (6456-01-5)

Guidance literature:

With hydrogenchloride; In methanol; for 1h; Reflux;

DOI:10.1007/s11172-009-0348-0

Reference yield: 44.0%

phenythoin (57-41-0) + methyl iodide (74-88-4) → 3-methyl-5,5-diphenyl-imidazolidine-2,4-dione (4224-00-4) + 1,3-dimethyl-5,5-diphenylhydantoin (6456-01-5)

Guidance literature:

phenythoin; With 18-crown-6 ether; potassium tert-butylate; In tetrahydrofuran; at 20 ℃; for 0.05h;

methyl iodide; In tetrahydrofuran; at 20 ℃; for 0.0833333h;

DOI:10.1248/CPB.C20-00857

upstream raw materials:

1,3-dimethyl-4,5-diphenyl-4,5-dihydroxyimidazolidin-2-one

1,1-Dimethylurea

Benzilic acid

benzil

Downstream raw materials:

3-methyl-5,5-diphenyl-imidazolidine-2,4-dione

1,3-dimethyl-5,5-diphenyl-2-thioxo-imidazolidin-4-one

1,3-Dimethyl-5,5-diphenyl-dithiohydantoin