BzMIMBr

Base Information

• Chemical Name: BzMIMBr
• CAS No.: 65039-11-4
• Molecular Formula: C11H13N2.Br
• Molecular Weight: 253.142
• Mol file: 65039-11-4.mol

Synonyms:

Chemical Property of BzMIMBr

Chemical Property:

• Melting Point: 173 °C
• PSA: 8.81000
• LogP: -1.63510

Purity/Quality:

97% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of BzMIMBr

There total 3 articles about BzMIMBr which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

1-methyl-1H-imidazole (616-47-7) + benzyl chloride (100-44-7) → 3-benzyl-1-methylimidazolium bromide (65039-11-4)

Guidance literature:

With potassium bromide; In acetonitrile; for 24h; Inert atmosphere;

DOI:10.1016/j.jorganchem.2013.01.016

Reference yield: 73.0%

1-methyl-1H-imidazole (616-47-7) + Benzoyl bromide (618-32-6) → 3-benzyl-1-methylimidazolium bromide (65039-11-4)

Guidance literature:

In toluene; for 24h; Reflux;

DOI:10.1039/d1ra07231e

Reference yield:

1-methyl-1H-imidazole (616-47-7) + N-benzylpyridinium bromide (2589-31-3) → pyridine (110-86-1) + 3-benzyl-1-methylimidazolium bromide (65039-11-4)

Guidance literature:

In [D₃]acetonitrile; at 150 ℃; for 0.5h; Microwave irradiation;

DOI:10.1002/asia.201500604

upstream raw materials:

1-methyl-1H-imidazole

benzyl chloride

N-benzylpyridinium bromide

Benzoyl bromide

Downstream raw materials:

3-benzyl-1-methylimidazolium octylsulfate

potassium formate

methylamine

benzylamine