1H-Germole, 2,5-dihydro-3-methyl-1,1-diphenyl-

Base Information

Chemical Name:1H-Germole, 2,5-dihydro-3-methyl-1,1-diphenyl-
CAS No.:65042-88-8
Molecular Formula:C₁₇H₁₈Ge
Molecular Weight:294.92
Hs Code.:

Synonyms:

Suppliers and Price of 1H-Germole, 2,5-dihydro-3-methyl-1,1-diphenyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of 1H-Germole, 2,5-dihydro-3-methyl-1,1-diphenyl-

Chemical Property:

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

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Technology Process of 1H-Germole, 2,5-dihydro-3-methyl-1,1-diphenyl-

There total 3 articles about 1H-Germole, 2,5-dihydro-3-methyl-1,1-diphenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 27.0%

: 111655-78-8
bis(trimethylsilyl)diphenylgermane

: 513-81-5
2,3-dimethyl-buta-1,3-diene

: 78-79-5,9003-31-0
isoprene

: 65042-88-8
1,1-diphenyl-4-methyl-1-germacyclopent-3-ene

: 5764-69-2
1,1-diphenyl-3,4-dimethyl-1-germacyclopent-3-ene

Guidance literature:: In cyclohexane; byproducts: Me3SiSiMe3; Irradiation (UV/VIS); Solns. of (Me3Si)2GePh2 in cyclohexane readily undergo photolysis to diphenylgermylene and hexamethyldisilane, when irradiated by an array of low pressure Hg lamps through quartz vessels.; The yields are obtained by (1)H NMR integration.;
DOI:10.1016/0022-328X(88)89115-0

Reference yield:

: 5764-69-2
1,1-diphenyl-3,4-dimethyl-1-germacyclopent-3-ene

: 78-79-5,9003-31-0
isoprene

: 65042-88-8
1,1-diphenyl-4-methyl-1-germacyclopent-3-ene

Guidance literature:: In Cyclohexane-d12; byproducts: 2,3-dimethyl-1,3-butadiene; Irradiation (UV/VIS); photolysis of a soln. of germanium compd. in C6D12 with isoprene at 254 nm;
DOI:10.1021/ja046308y

Reference yield:

: 5764-69-2
1,1-diphenyl-3,4-dimethyl-1-germacyclopent-3-ene

: 65042-88-8
1,1-diphenyl-4-methyl-1-germacyclopent-3-ene

Guidance literature:: With isoprene; In cyclohexane-d12; byproducts: 2,3-dimethyl-1,3-butadiene; Irradiation (UV/VIS); under Ar; soln. of Ge compd. in cyclohexane-d12 contg. isoprene subjected to photolysis at 25 and 51°C; not isolated; monitored by (1)H NMR and mass spectra; Ph2GeC4H5CH3, CH3C(CH2)C(CH2)CH3 and Ge-contg. oligomeric compds. obtained;
DOI:10.1021/om900791e