3,4-Dimethyl-1,1-diphenyl-2,5-dihydro-1H-germole

Base Information

Chemical Name:3,4-Dimethyl-1,1-diphenyl-2,5-dihydro-1H-germole
CAS No.:5764-69-2
Molecular Formula:C18H20Ge
Molecular Weight:308.947
Hs Code.:
DSSTox Substance ID:DTXSID60532150
Nikkaji Number:J1.388.356D
Wikidata:Q82404537

Synonyms:5764-69-2;3,4-Dimethyl-1,1-diphenyl-2,5-dihydro-1H-germole;DTXSID60532150;3,4-dimethyl-1,1-diphenylger-macyclopent-3-ene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3,4-Dimethyl-1,1-diphenyl-2,5-dihydro-1H-germole

Chemical Property:

Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:2
Exact Mass:310.0776784
Heavy Atom Count:19
Complexity:309

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC1=C(C[Ge](C1)(C2=CC=CC=C2)C3=CC=CC=C3)C

Technology Process of 3,4-Dimethyl-1,1-diphenyl-2,5-dihydro-1H-germole

There total 15 articles about 3,4-Dimethyl-1,1-diphenyl-2,5-dihydro-1H-germole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 111655-78-8
bis(trimethylsilyl)diphenylgermane

: 513-81-5
2,3-dimethyl-buta-1,3-diene

: 1450-14-2
1,1,1,2,2,2-hexamethyldisilane

: 768-32-1
trimethylphenylsilane

: 5764-69-2
1,1-diphenyl-3,4-dimethyl-1-germacyclopent-3-ene

Guidance literature:: In pentane; Irradiation (UV/VIS); (N2), 1 h irradiated; gas chromatography; elem. anal., NMR, mass. spectra;
DOI:10.1021/om00054a046

Reference yield: 53.0%

: 37044-16-9
tetraphenyldigermanium dichloride

: 513-81-5
2,3-dimethyl-buta-1,3-diene

: 5764-69-2
1,1-diphenyl-3,4-dimethyl-1-germacyclopent-3-ene

: 1613-66-7
dichlorodiphenylgermane

Guidance literature:: In neat (no solvent); Ge deriv. heating with a large excess of organic reagent in a sealed tube at 130°C for 4 h, concg. in vacuo; identified by high-pressure chromy. and NMR spectra;
DOI:10.1016/0022-328X(84)85145-1

Reference yield: 46.0%

: 53421-59-3
1,1,1,3,3,3-hexamethyl-2,2-diphenyl-trigermane

: 513-81-5
2,3-dimethyl-buta-1,3-diene

: 993-52-2
hexamethyldigermane

: 5764-69-2
1,1-diphenyl-3,4-dimethyl-1-germacyclopent-3-ene

Guidance literature:: In cyclohexane; Irradiation (UV/VIS); 110-W low pressure Hg arc lamp, under Ar, room temp.; GC-MS; Kinetics;
DOI:10.1016/0022-328X(89)87334-6