Silane, (3-bromo-2,6-difluorophenyl)triethyl-

Base Information

Chemical Name:Silane, (3-bromo-2,6-difluorophenyl)triethyl-
CAS No.:651027-03-1
Molecular Formula:C12H17BrF2Si
Molecular Weight:307.253
Hs Code.:
DSSTox Substance ID:DTXSID70463527
Wikidata:Q82288423

Synonyms:651027-03-1;Silane, (3-bromo-2,6-difluorophenyl)triethyl-;SCHEMBL12350311;DTXSID70463527

Suppliers and Price of Silane, (3-bromo-2,6-difluorophenyl)triethyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of Silane, (3-bromo-2,6-difluorophenyl)triethyl-

Chemical Property:

Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:4
Exact Mass:306.02510
Heavy Atom Count:16
Complexity:213

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC[Si](CC)(CC)C1=C(C=CC(=C1F)Br)F

Technology Process of Silane, (3-bromo-2,6-difluorophenyl)triethyl-

There total 4 articles about Silane, (3-bromo-2,6-difluorophenyl)triethyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 348-57-2
2,4-difluorobromobenzene

: 994-30-9
triethylsilyl chloride

: 651027-03-1
(3-bromo-2,6-difluorophenyl)triethylsilane

Guidance literature:: 2,4-difluorobromobenzene; With lithium diisopropyl amide; In tetrahydrofuran; at -78 ℃; for 1h;

triethylsilyl chloride; In tetrahydrofuran; at -78 ℃; for 2h;

Reference yield: 92.0%

: 651027-02-0
1-triethylsilyl-2,6-difluorobenzene

: 651027-03-1
(3-bromo-2,6-difluorophenyl)triethylsilane

Guidance literature:: With bromine; sec.-butyllithium; In tetrahydrofuran; cyclohexane; for 0.75h;
DOI:10.1002/ejoc.200300354

Reference yield:

: 994-30-9
triethylsilyl chloride

: 651027-03-1
(3-bromo-2,6-difluorophenyl)triethylsilane

Guidance literature:: Multi-step reaction with 2 steps

1: 89 percent / butyllithium / hexane; tetrahydrofuran / -75 °C

2: 92 percent / sec-butyllithium; bromine / cyclohexane; tetrahydrofuran / 0.75 h

With n-butyllithium; bromine; sec.-butyllithium; In tetrahydrofuran; hexane; cyclohexane;
DOI:10.1002/ejoc.200300354