Silane, (2,6-difluorophenyl)triethyl-

Base Information

• Chemical Name: Silane, (2,6-difluorophenyl)triethyl-
• CAS No.: 651027-02-0
• Molecular Formula: C12H18F2Si
• Molecular Weight: 228.357
• DSSTox Substance ID: DTXSID00465817
• Nikkaji Number: J2.011.014G
• Wikidata: Q82292061

Synonyms:Silane, (2,6-difluorophenyl)triethyl-;651027-02-0;DTXSID00465817

Chemical Property of Silane, (2,6-difluorophenyl)triethyl-

Chemical Property:

• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 4
• Exact Mass: 228.11458343
• Heavy Atom Count: 15
• Complexity: 174

Purity/Quality:

85.0-99.8% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC[Si](CC)(CC)C1=C(C=CC=C1F)F

Technology Process of Silane, (2,6-difluorophenyl)triethyl-

There total 1 articles about Silane, (2,6-difluorophenyl)triethyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

triethylsilyl chloride (994-30-9) + 1,3-Difluorobenzene (372-18-9) → 1-triethylsilyl-2,6-difluorobenzene (651027-02-0)

Guidance literature:

With n-butyllithium; In tetrahydrofuran; hexane; at -75 ℃;

DOI:10.1002/ejoc.200300354

Reference yield: 92.0%

1-triethylsilyl-2,6-difluorobenzene (651027-02-0) → (3-bromo-2,6-difluorophenyl)triethylsilane (651027-03-1)

Guidance literature:

With bromine; sec.-butyllithium; In tetrahydrofuran; cyclohexane; for 0.75h;

DOI:10.1002/ejoc.200300354

Reference yield: 89.0%

carbon dioxide (124-38-9,18923-20-1) + 1-triethylsilyl-2,6-difluorobenzene (651027-02-0) → 2,4-difluoro-3-(triethylsilyl)benzoic acid (651027-06-4)

Guidance literature:

With sec.-butyllithium; In tetrahydrofuran; cyclohexane; for 0.75h;

DOI:10.1002/ejoc.200300354

upstream raw materials:

triethylsilyl chloride

1,3-Difluorobenzene

Downstream raw materials:

2,4-difluoro-3-(triethylsilyl)benzoic acid

(3-bromo-2,6-difluorophenyl)triethylsilane

3,5-difluorobromobenzene

3,5-difluorobenzoic acid

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