2-Furancarboxylic acid, 5-[[[6-[[(1R)-2-[[(1,1-dimethylethyl)dimethylsilyl]oxy]-1-methylethyl]amino] -2-[(phenylmethyl)thio]-4-pyrimidinyl]amino]sulfonyl]-, methyl ester

Base Information

Chemical Name:2-Furancarboxylic acid, 5-[[[6-[[(1R)-2-[[(1,1-dimethylethyl)dimethylsilyl]oxy]-1-methylethyl]amino] -2-[(phenylmethyl)thio]-4-pyrimidinyl]amino]sulfonyl]-, methyl ester
CAS No.:654074-55-2
Molecular Formula:C26H36N4O6S2Si
Molecular Weight:592.813
Hs Code.:

2-Furancarboxylic acid,
5-[[[6-[[(1R)-2-[[(1,1-dimethylethyl)dimethylsilyl]oxy]-1-methylethyl]amino]
-2-[(phenylmethyl)thio]-4-pyrimidinyl]amino]sulfonyl]-, methyl ester

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Chemical Property of 2-Furancarboxylic acid, 5-[[[6-[[(1R)-2-[[(1,1-dimethylethyl)dimethylsilyl]oxy]-1-methylethyl]amino] -2-[(phenylmethyl)thio]-4-pyrimidinyl]amino]sulfonyl]-, methyl ester

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Technology Process of 2-Furancarboxylic acid, 5-[[[6-[[(1R)-2-[[(1,1-dimethylethyl)dimethylsilyl]oxy]-1-methylethyl]amino] -2-[(phenylmethyl)thio]-4-pyrimidinyl]amino]sulfonyl]-, methyl ester

There total 4 articles about 2-Furancarboxylic acid, 5-[[[6-[[(1R)-2-[[(1,1-dimethylethyl)dimethylsilyl]oxy]-1-methylethyl]amino] -2-[(phenylmethyl)thio]-4-pyrimidinyl]amino]sulfonyl]-, methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 654072-59-0
2-(benzylthio)-N-((1R)-2-{[tert-butyl(dimethyl)silyl]oxy}-1-methylethyl)pyrimidine-4,6-diamine

: 69816-05-3
2-furancarboxylic acid 5-(chlorosulfonyl) methyl ester

: 654074-55-2
methyl 5-[({2-(benzylthio)-6-[((1R)-2-{[tert-butyl(dimethyl)silyl]oxy}-1-methylethyl)amino]pyrimidin-4-yl}amino)sulfonyl]-2-furoate

Guidance literature:: With pyridine; dmap; for 36h;

Reference yield:

: (2R)-2-{[6-amino-2-(benzylthio)pyrimidin-4-yl]amino}propan-1-ol

: 654074-55-2
methyl 5-[({2-(benzylthio)-6-[((1R)-2-{[tert-butyl(dimethyl)silyl]oxy}-1-methylethyl)amino]pyrimidin-4-yl}amino)sulfonyl]-2-furoate

Guidance literature:: Multi-step reaction with 2 steps

1: 1H-imidazole / DMF (N,N-dimethyl-formamide) / 48 h

2: pyridine / dmap / 36 h

With pyridine; 1H-imidazole; dmap; In DMF (N,N-dimethyl-formamide);

Reference yield:

: 18162-48-6
tert-butyldimethylsilyl chloride

: 654074-55-2
methyl 5-[({2-(benzylthio)-6-[((1R)-2-{[tert-butyl(dimethyl)silyl]oxy}-1-methylethyl)amino]pyrimidin-4-yl}amino)sulfonyl]-2-furoate

Guidance literature:: Multi-step reaction with 2 steps

1: 1H-imidazole / DMF (N,N-dimethyl-formamide) / 48 h

2: pyridine / dmap / 36 h

With pyridine; 1H-imidazole; dmap; In DMF (N,N-dimethyl-formamide);