1-phenyl-N-tritylsulfanylethanimine

Base Information

Chemical Name:1-phenyl-N-tritylsulfanylethanimine
CAS No.:86864-37-1
Molecular Formula:C27H23NS
Molecular Weight:393.5432
Hs Code.:
NSC Number:378996
DSSTox Substance ID:DTXSID00421690

Synonyms:86864-37-1;1-phenyl-N-tritylsulfanylethanimine;NSC378996;DTXSID00421690;NSC-378996

Suppliers and Price of 1-phenyl-N-tritylsulfanylethanimine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of 1-phenyl-N-tritylsulfanylethanimine

Chemical Property:

Vapor Pressure:9.94E-11mmHg at 25°C
Boiling Point:528.6°Cat760mmHg
Flash Point:273.5°C
Density:1.04g/cm³
XLogP3:7
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:6
Exact Mass:393.15512091
Heavy Atom Count:29
Complexity:457

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(=NSC(C1=CC=CC=C1)(C2=CC=CC=C2)C3=CC=CC=C3)C4=CC=CC=C4
Isomeric SMILES:C/C(=N\SC(C1=CC=CC=C1)(C2=CC=CC=C2)C3=CC=CC=C3)/C4=CC=CC=C4

Technology Process of 1-phenyl-N-tritylsulfanylethanimine

There total 3 articles about 1-phenyl-N-tritylsulfanylethanimine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: 38499-08-0
Triphenylmethanesulfenamide

: 98-86-2
acetophenone

: 86864-37-1
Acetophenone tritylsulfenimine

Guidance literature:: With calcium hydride; 3 A molecular sieve; pyridinium p-toluenesulfonate; magnesium sulfate; In dichloromethane; for 72h; Heating;
DOI:10.1021/jo00168a031

Reference yield:

: 3695-77-0
triphenylmethanethiol

: 86864-37-1
Acetophenone tritylsulfenimine

Guidance literature:: Multi-step reaction with 3 steps

1: 88 percent / Sulfuryl chloride / toluene; diethyl ether / 2 h / 0 °C

2: 78 percent / 29 percent NH₄OH/H₂O / CH₂Cl₂ / 0 °C

3: 59 percent / 3-Angstroem molecular sieves, CaH₂; Pyridinium p-toluenesulfonate, (PPTS)/anhydr. MgSO₄ / CH₂Cl₂ / 72 h / Heating

With ammonium hydroxide; sulfuryl dichloride; calcium hydride; 3 A molecular sieve; water; pyridinium p-toluenesulfonate; magnesium sulfate; In diethyl ether; dichloromethane; toluene;
DOI:10.1021/jo00168a031

Reference yield:

: 24165-03-5
tritylsulfenyl chloride

: 86864-37-1
Acetophenone tritylsulfenimine

Guidance literature:: Multi-step reaction with 2 steps

1: 78 percent / 29 percent NH₄OH/H₂O / CH₂Cl₂ / 0 °C

2: 59 percent / 3-Angstroem molecular sieves, CaH₂; Pyridinium p-toluenesulfonate, (PPTS)/anhydr. MgSO₄ / CH₂Cl₂ / 72 h / Heating

With ammonium hydroxide; calcium hydride; 3 A molecular sieve; water; pyridinium p-toluenesulfonate; magnesium sulfate; In dichloromethane;
DOI:10.1021/jo00168a031