PHENYL(3,4,5-TRIMETHOXYPHENYL)METHANOL

Base Information

Chemical Name:PHENYL(3,4,5-TRIMETHOXYPHENYL)METHANOL
CAS No.:6590-62-1
Molecular Formula:C16H18O4
Molecular Weight:274.317
Hs Code.:
Mol file:6590-62-1.mol

Synonyms:3,4,5-Trimethoxybenzhydrol;3,4,5-Trimethoxy-benzhydrol;phenyl-(3,4,5-trimethoxyphenyl)-methanol;phenyl (3,4,5-trimethoxyphenyl)methanol;

Suppliers and Price of PHENYL(3,4,5-TRIMETHOXYPHENYL)METHANOL

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Crysdot
Phenyl(3,4,5-trimethoxyphenyl)methanol 97%
1g
$ 452.00

American Custom Chemicals Corporation
PHENYL(3,4,5-TRIMETHOXYPHENYL)METHANOL 95.00%
5MG
$ 503.29

Total 4 raw suppliers

Chemical Property of PHENYL(3,4,5-TRIMETHOXYPHENYL)METHANOL

Chemical Property:

PSA：47.92000
LogP:2.79410

Purity/Quality:

97% ^*data from raw suppliers

Phenyl(3,4,5-trimethoxyphenyl)methanol 97% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of PHENYL(3,4,5-TRIMETHOXYPHENYL)METHANOL

There total 9 articles about PHENYL(3,4,5-TRIMETHOXYPHENYL)METHANOL which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 86-81-7
3,4,5-trimethoxy-benzaldehyde

: 98-80-6
phenylboronic acid

: 6590-62-1
(3,4,5-trimethoxyphenyl)(phenyl)methanol

Guidance literature:: With potassium tert-butylate; RhCl(COD)(1,3-dialkyl-3,4,5,6-tetrahydropyrimidin-2-ylidene); In 1,2-dimethoxyethane; water; at 80 ℃; for 7h;
DOI:10.1016/j.jorganchem.2005.07.085

Reference yield: 92.0%

: 2675-79-8
1-bromo-3,4,5-trimethoxybenzene

: 100-52-7
benzaldehyde

: 6590-62-1
(3,4,5-trimethoxyphenyl)(phenyl)methanol

Guidance literature:: 1-bromo-3,4,5-trimethoxybenzene; With secBu₂Mg LiCl; In tetrahydrofuran; at 25 ℃; for 2h;

benzaldehyde; In tetrahydrofuran; at 0 ℃; for 0.0833333h;
DOI:10.1002/anie.200502220

Reference yield: 87.0%

: 86-81-7
3,4,5-trimethoxy-benzaldehyde

: 100-58-3
phenylmagnesium bromide

: 6590-62-1
(3,4,5-trimethoxyphenyl)(phenyl)methanol

Guidance literature:: 3,4,5-trimethoxy-benzaldehyde; phenylmagnesium bromide; In tetrahydrofuran; diethyl ether; at 0 - 20 ℃; for 8h; Inert atmosphere;

With water; In tetrahydrofuran; diethyl ether; Inert atmosphere;
DOI:10.1016/j.bmc.2009.08.011