4-Methyl-5-nitrobenzene-1,2-diaMine

Base Information

Chemical Name:4-Methyl-5-nitrobenzene-1,2-diaMine
CAS No.:65958-37-4
Molecular Formula:C7H9N3O2
Molecular Weight:167.167
Hs Code.:2921590090
Mol file:65958-37-4.mol

Synonyms:4-nitro-5-methyl-1,2-phenylenediamine;1H-Indole,4-methyl-5-nitro;4-Methyl-5-nitro-o-phenylendiamin;4-methyl-5-nitroindole;4-methyl-5-nitro-o-phenylenediamine;

Suppliers and Price of 4-Methyl-5-nitrobenzene-1,2-diaMine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Crysdot
4-Methyl-5-nitrobenzene-1,2-diamine 95+%
1g
$ 488.00

Crysdot
4-Methyl-5-nitrobenzene-1,2-diamine 95+%
250mg
$ 205.00

Crysdot
4-Methyl-5-nitrobenzene-1,2-diamine 95+%
100mg
$ 126.00

Ambeed
4-Methyl-5-nitrobenzene-1,2-diamine 95+%
250mg
$ 92.00

Ambeed
4-Methyl-5-nitrobenzene-1,2-diamine 95+%
100mg
$ 56.00

Ambeed
4-Methyl-5-nitrobenzene-1,2-diamine 95+%
1g
$ 237.00

Alichem
4-Methyl-5-nitrobenzene-1,2-diamine
1g
$ 611.52

Alichem
4-Methyl-5-nitrobenzene-1,2-diamine
250mg
$ 242.05

Alichem
4-Methyl-5-nitrobenzene-1,2-diamine
100mg
$ 155.82

AK Scientific
4-Methyl-5-nitrobenzene-1,2-diamine
1g
$ 379.00

Total 9 raw suppliers

Chemical Property of 4-Methyl-5-nitrobenzene-1,2-diaMine

Chemical Property:

Melting Point:146-147 °C
Boiling Point:405.0±40.0 °C(Predicted)
PKA:2.55±0.10(Predicted)
PSA：97.86000
Density:1.369±0.06 g/cm3(Predicted)
LogP:2.75320

Purity/Quality:

97% ^*data from raw suppliers

4-Methyl-5-nitrobenzene-1,2-diamine 95+% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 4-Methyl-5-nitrobenzene-1,2-diaMine

There total 6 articles about 4-Methyl-5-nitrobenzene-1,2-diaMine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 5267-27-6
5-amino-2,4-dinitrotoluene

: 65958-37-4
4-methyl-5-nitrobenzene-1,2-diamine

Guidance literature:: With sodium sulfide; water; In ethanol; at 20 - 100 ℃; for 2h; Inert atmosphere;
DOI:10.1016/j.bmc.2015.11.035

Reference yield: 38.0%

: 496-72-0
4-methyl-1,2-diaminobenzene

: 65958-37-4
4-methyl-5-nitrobenzene-1,2-diamine

Guidance literature:: With hydrogen sulfide; ammonia; In water; at 45 - 55 ℃; for 0.75h;

Reference yield:

: 89-62-3
4-methyl-2-nitroaniline

: 65958-37-4
4-methyl-5-nitrobenzene-1,2-diamine

Guidance literature:: Multi-step reaction with 2 steps

1: Raney Ni, H₂ / ethanol

2: 38 percent / NH₃, H₂S / H₂O / 0.75 h / 45 - 55 °C

With hydrogen sulfide; ammonia; hydrogen; nickel; In ethanol; water;