N-(2-hydroxyethyl)methanesulfonamide

Base Information

• Chemical Name: N-(2-hydroxyethyl)methanesulfonamide
• CAS No.: 6601-38-3
• Molecular Formula: C3H9NO3S
• Molecular Weight: 139.17300
• European Community (EC) Number: 854-865-1
• DSSTox Substance ID: DTXSID001290797

Synonyms:N-(2-hydroxyethyl)methanesulfonamide;6601-38-3;SCHEMBL48208;DTXSID001290797;MFCD11611046;AKOS008030902;BS-12890;CS-0256790;EN300-65217;Z57801016

Chemical Property of N-(2-hydroxyethyl)methanesulfonamide

Chemical Property:

• PSA: 74.78000
• LogP: -0.00040
• XLogP3: -1.4
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 3
• Exact Mass: 139.03031432
• Heavy Atom Count: 8
• Complexity: 133

Purity/Quality:

95% ^*data from raw suppliers

N-(2-hydroxyethyl)methanesulfonamide ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CS(=O)(=O)NCCO

Technology Process of N-(2-hydroxyethyl)methanesulfonamide

There total 1 articles about N-(2-hydroxyethyl)methanesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

ethanolamine (141-43-5) + methanesulfonyl chloride (124-63-0) → N-(2-hydroxyethyl)methanesulfonamide (6601-38-3)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 0 - 20 ℃;

Reference yield: 69.0%

N-(2-hydroxyethyl)methanesulfonamide (6601-38-3) + N-[6-Chloro-5-(2-methoxyphenoxy)-2-(2-pyrimidinyl)-4-pyrimidinyl]-2-phenylethenesulfonamide (351019-39-1) → (E)-2-Phenyl-ethenesulfonic acid [6-(2-methanesulfonylamino-ethoxy)-5-(2-methoxy-phenoxy)-[2,2']bipyrimidinyl-4-yl]-amide

Guidance literature:

N-(2-hydroxyethyl)methanesulfonamide; With sodium hydride; In N,N-dimethyl-formamide; at 20 ℃; for 0.5h;

N-[6-Chloro-5-(2-methoxyphenoxy)-2-(2-pyrimidinyl)-4-pyrimidinyl]-2-phenylethenesulfonamide; In N,N-dimethyl-formamide; at 20 ℃; for 3h;

DOI:10.1248/cpb.49.606

upstream raw materials:

ethanolamine

methanesulfonyl chloride

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