Benzenesulfenamide, N,N-diethyl-

Base Information

• Chemical Name: Benzenesulfenamide, N,N-diethyl-
• CAS No.: 6667-19-2
• Molecular Formula: C10H15NS
• Molecular Weight: 181.302
• DSSTox Substance ID: DTXSID10457905
• Nikkaji Number: J1.208.681D
• Wikidata: Q82280960
• Mol file: 6667-19-2.mol

Synonyms:Benzenesulfenamide, N,N-diethyl-;6667-19-2;Phenylthiodiethylamine;N,N-diethylphenylsulfenamide;SCHEMBL18602990;DTXSID10457905;N,N-Diethyl-S-phenyl-thiohydroxylamine

Chemical Property of Benzenesulfenamide, N,N-diethyl-

Chemical Property:

• XLogP3: 3
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 4
• Exact Mass: 181.09252066
• Heavy Atom Count: 12
• Complexity: 106

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: CCN(CC)SC1=CC=CC=C1

Technology Process of Benzenesulfenamide, N,N-diethyl-

There total 16 articles about Benzenesulfenamide, N,N-diethyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

thiophenol (108-98-5) + diethylamine (109-89-7) → benzenenesulfenyl dimethylamine (6667-19-2)

Guidance literature:

With [2,2]bipyridinyl; copper(l) iodide; oxygen; In dimethyl sulfoxide; at 60 ℃; for 18h;

DOI:10.1002/ejoc.201000167

Reference yield: 82.0%

C14H19S(1+) + diethylamine (109-89-7) → benzenenesulfenyl dimethylamine (6667-19-2)

Guidance literature:

C₁₄H₁₉S⁽¹⁺⁾; With hexadec-8-yne; tetrabutylammonium tetrafluoroborate; In dichloromethane; at -78 ℃; Inert atmosphere; Electrochemical reaction;

diethylamine; In dichloromethane; at -78 - 20 ℃; for 1h; Inert atmosphere; Electrochemical reaction;

DOI:10.24820/ark.5550190.p010.302

Reference yield: 75.0%

diethylamine (109-89-7) + benzenesulfenyl chloride (931-59-9) → benzenenesulfenyl dimethylamine (6667-19-2)

Guidance literature:

In diethyl ether; at 0 ℃; for 1h;

DOI:10.1016/0040-4020(96)00487-5

upstream raw materials:

phenylsulfenyl bromide

diethylamine

benzenesulfenyl thiocyanate

diethyl ether

Downstream raw materials:

benzenesulfenyl chloride

diphenyl sulfide

diethylamine

Cyano-phenylsulfanyl-acetic acid ethyl ester