6-Vinyl-2,3-dihydrobenzo[b][1,4]dioxine

Base Information

Chemical Name:6-Vinyl-2,3-dihydrobenzo[b][1,4]dioxine
CAS No.:67200-27-5
Molecular Formula:C10H10O2
Molecular Weight:162.188
Hs Code.:
DSSTox Substance ID:DTXSID60458265
Wikidata:Q82281469

Synonyms:6-vinyl-2,3-dihydrobenzo[b][1,4]dioxine;67200-27-5;6-ethenyl-2,3-dihydro-1,4-benzodioxine;6-vinyl-1,4-benzodioxane;SCHEMBL3775431;DTXSID60458265;UYDKUTIEPBVQAK-UHFFFAOYSA-N;AKOS013992628;2,3-dihydro-6-vinylbenzo[1,4]dioxin;6-Vinyl-2,3-dihydro-benzo[1,4]dioxine;EN300-1243648;J-519005

Suppliers and Price of 6-Vinyl-2,3-dihydrobenzo[b][1,4]dioxine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Crysdot
6-Vinyl-2,3-dihydrobenzo[b][1,4]dioxine 95+%
1g
$ 772.00

Chemenu
6-vinyl-2,3-dihydrobenzo[b][1,4]dioxine 95%
1g
$ 729.00

American Custom Chemicals Corporation
6-VINYL-2,3-DIHYDROBENZO[B][1,4]DIOXINE 95.00%
5MG
$ 500.98

Alichem
6-Vinyl-2,3-dihydrobenzo[b][1,4]dioxine
1g
$ 659.40

Total 6 raw suppliers

Chemical Property of 6-Vinyl-2,3-dihydrobenzo[b][1,4]dioxine

Chemical Property:

Boiling Point:98-101 °C(Press: 3 Torr)
PSA：18.46000
Density:1.123±0.06 g/cm3(Predicted)
LogP:2.10080
XLogP3:2.8
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:1
Exact Mass:162.068079557
Heavy Atom Count:12
Complexity:167

Purity/Quality:

99% ^*data from raw suppliers

6-Vinyl-2,3-dihydrobenzo[b][1,4]dioxine 95+% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C=CC1=CC2=C(C=C1)OCCO2

Technology Process of 6-Vinyl-2,3-dihydrobenzo[b][1,4]dioxine

There total 6 articles about 6-Vinyl-2,3-dihydrobenzo[b][1,4]dioxine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 1779-49-3
Methyltriphenylphosphonium bromide

: 29668-44-8
2,3-dihydro-benzo[1,4]dioxin-6-carbaldehyde

: 67200-27-5
6-vinyl-2,3-dihydrobenzo[b][1,4]dioxine

Guidance literature:: Methyltriphenylphosphonium bromide; With n-butyllithium; In tetrahydrofuran; at 0 ℃; for 0.25h; Inert atmosphere;

2,3-dihydro-benzo[1,4]dioxin-6-carbaldehyde; In tetrahydrofuran; for 8h;

Reference yield: 63.0%

: 2768-02-7
(vinyl)trimethoxylsilane

: 52287-51-1
6-bromo-1,4-benzodioxane

: 67200-27-5
6-vinyl-2,3-dihydrobenzo[b][1,4]dioxine

Guidance literature:: (vinyl)trimethoxylsilane; 6-bromo-1,4-benzodioxane; With (1,2-dimethoxyethane)dichloronickel(II); tetrabutylammonium triphenyldifluorosilicate; In N,N-dimethyl acetamide; Inert atmosphere;

(vinyl)trimethoxylsilane;
DOI:10.1055/a-1379-1584