methyl 4-{(E)-[(4-methoxyphenyl)imino]methyl}benzoate

Base Information

Chemical Name:methyl 4-{(E)-[(4-methoxyphenyl)imino]methyl}benzoate
CAS No.:673855-94-2
Molecular Formula:C16H15NO3
Molecular Weight:269.3
Hs Code.:
DSSTox Substance ID:DTXSID90586065
Nikkaji Number:J2.785.608J

Synonyms:673855-94-2;methyl 4-{(E)-[(4-methoxyphenyl)imino]methyl}benzoate;Benzoic acid, 4-[[(4-methoxyphenyl)imino]methyl]-, methyl ester;SCHEMBL11438344;DTXSID90586065;STK882434;AKOS002198691;MCULE-1543398109

Suppliers and Price of methyl 4-{(E)-[(4-methoxyphenyl)imino]methyl}benzoate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of methyl 4-{(E)-[(4-methoxyphenyl)imino]methyl}benzoate

Chemical Property:

XLogP3:3.6
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:5
Exact Mass:269.10519334
Heavy Atom Count:20
Complexity:327

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=CC=C(C=C1)N=CC2=CC=C(C=C2)C(=O)OC

Technology Process of methyl 4-{(E)-[(4-methoxyphenyl)imino]methyl}benzoate

There total 2 articles about methyl 4-{(E)-[(4-methoxyphenyl)imino]methyl}benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 104-94-9
4-methoxy-aniline

: 1571-08-0
methyl 4-formylbenzoate

: 673855-94-2
methyl 4-{[(4-methoxyphenyl)imino]methyl}benzoate

Guidance literature:: In tetrahydrofuran; at 20 ℃; for 0.0833333h;
DOI:10.1246/cl.160217

Reference yield: 83.0%

: 104-94-9
4-methoxy-aniline

: 105-45-3
acetoacetic acid methyl ester

: 1571-08-0
methyl 4-formylbenzoate

: 123958-76-9
C₁₂H₁₅NO₃

: 673855-94-2
methyl 4-{[(4-methoxyphenyl)imino]methyl}benzoate

Guidance literature:: With indium(III) chloride; In acetonitrile; at 20 ℃;
DOI:10.1055/s-0028-1083182

Reference yield: 99.0%

: 673855-94-2
methyl 4-{[(4-methoxyphenyl)imino]methyl}benzoate

: 140-89-6
potassium ethyl xanthogenate

: 75-36-5
acetyl chloride

: methyl (RS)-4-{[(ethoxycarbonothioyl)thio][N-(4-methoxyphenyl)acetamido]methyl}benzoate

Guidance literature:: methyl 4-{[(4-methoxyphenyl)imino]methyl}benzoate; acetyl chloride; In tetrahydrofuran; at 0 - 20 ℃; for 3h; Inert atmosphere; Schlenk technique; Green chemistry;

potassium ethyl xanthogenate; In tetrahydrofuran; at 0 - 20 ℃; for 2h; Inert atmosphere; Schlenk technique; Green chemistry;
DOI:10.1055/s-0036-1589050