N,N,3-Trimethylbutanethioamide

Base Information

Chemical Name:N,N,3-Trimethylbutanethioamide
CAS No.:67797-33-5
Molecular Formula:C7H15NS
Molecular Weight:145.269
Hs Code.:
DSSTox Substance ID:DTXSID40497814
Wikidata:Q82347578

Synonyms:N,N,3-Trimethylbutanethioamide;67797-33-5;SCHEMBL14611629;DTXSID40497814

Suppliers and Price of N,N,3-Trimethylbutanethioamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of N,N,3-Trimethylbutanethioamide

Chemical Property:

XLogP3:1.6
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:2
Exact Mass:145.09252066
Heavy Atom Count:9
Complexity:97.1

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(C)CC(=S)N(C)C

Technology Process of N,N,3-Trimethylbutanethioamide

There total 1 articles about N,N,3-Trimethylbutanethioamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 78175-62-9
3-Hydroxy-2-isopropyl-N,N-dimethyl-3-phenyl-thiobutyramide

: 67-64-1
acetone

: 43108-74-3
3-hydroxy-3-methyl-1-phenyl-1-butanone

: 67797-33-5
N,N-Dimethylisovalerothioamide

: 98-86-2
acetophenone

Guidance literature:: With lithium diisopropyl amide; Yield given. Multistep reaction. Yields of byproduct given; 1.) ether, -25 deg C, 12 h, 2.) ether, -60 deg C, 1 h;
DOI:10.1016/S0022-328X(00)86714-5

Reference yield:

: 67797-33-5
N,N-Dimethylisovalerothioamide

: 90421-14-0,90421-16-2
3,N,N-Trimethyl-2-(phenyl-trimethylsilanyloxy-methyl)-thiobutyramide

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) LDA / 1.) ether, -25 deg C

2: tetrabutylammonium fluoride / tetrahydrofuran

With lithium diisopropyl amide; tetrabutyl ammonium fluoride; In tetrahydrofuran;
DOI:10.1016/S0040-4039(00)88247-7

Reference yield:

: 67797-33-5
N,N-Dimethylisovalerothioamide

: 90421-14-0,90421-16-2
3,N,N-Trimethyl-2-(phenyl-trimethylsilanyloxy-methyl)-thiobutyramide

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) LDA / 1.) ether, -25 deg C

2: tetrabutylammonium fluoride / tetrahydrofuran

With lithium diisopropyl amide; tetrabutyl ammonium fluoride; In tetrahydrofuran;
DOI:10.1016/S0040-4039(00)88247-7