N-[(1E)-2,2,2-Trichloroethylidene]benzamide

Base Information

Chemical Name:N-[(1E)-2,2,2-Trichloroethylidene]benzamide
CAS No.:6780-37-6
Molecular Formula:C9H6Cl3NO
Molecular Weight:250.512
Hs Code.:
DSSTox Substance ID:DTXSID80493976
Nikkaji Number:J341.312H

Synonyms:6780-37-6;N-(benzoyl)trichloroacetaldimine;DTXSID80493976;N-[(1E)-2,2,2-Trichloroethylidene]benzamide

Suppliers and Price of N-[(1E)-2,2,2-Trichloroethylidene]benzamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of N-[(1E)-2,2,2-Trichloroethylidene]benzamide

Chemical Property:

XLogP3:3.3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:1
Exact Mass:248.951497
Heavy Atom Count:14
Complexity:229

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1=CC=C(C=C1)C(=O)N=CC(Cl)(Cl)Cl

Technology Process of N-[(1E)-2,2,2-Trichloroethylidene]benzamide

There total 7 articles about N-[(1E)-2,2,2-Trichloroethylidene]benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

: 25408-75-7
N,N'-dibenzoylsulfur diimide

: 75-87-6
chloral

: 6780-37-6
N-(benzoyl)trichloroacetaldimine

Guidance literature:: With aluminium trichloride; at 110 - 112 ℃;

Reference yield:

: 6798-35-2
N-(1,2,2,2-tetrachloroethyl)benzamide

: 6780-37-6
N-(benzoyl)trichloroacetaldimine

Guidance literature:: With triethylamine; In tetrahydrofuran;

Reference yield:

: 6316-07-0
N-(2,2,2-trichloro-1-hydroxyethyl)benzamide

: 6780-37-6
N-(benzoyl)trichloroacetaldimine

Guidance literature:: Multi-step reaction with 2 steps

1: SOCl₂ / benzene / 4 h / 80 °C

2: hydroquinone, Et₃N / benzene / 30 - 40 °C

With thionyl chloride; triethylamine; hydroquinone; In benzene;