1,4-Pentanediamine, N4-(6-methoxy-4,5-dimethyl-8-quinolinyl)-, (2Z)-2-butenedioate (1:1)

Base Information

Chemical Name:1,4-Pentanediamine, N4-(6-methoxy-4,5-dimethyl-8-quinolinyl)-, (2Z)-2-butenedioate (1:1)
CAS No.:76100-57-7
Molecular Formula:C₄H₄O₄*C₁₇H₂₅N₃O
Molecular Weight:403.478
Hs Code.:

Synonyms:1,4-Pentanediamine, N4-(6-methoxy-4,5-dimethyl-8-quinolinyl)-, (2Z)-2-butenedioate (1:1);(Z)-but-2-enedioic acid;4-N-(6-methoxy-4,5-dimethylquinolin-8-yl)pentane-1,4-diamine

Suppliers and Price of 1,4-Pentanediamine, N4-(6-methoxy-4,5-dimethyl-8-quinolinyl)-, (2Z)-2-butenedioate (1:1)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 0 raw suppliers

Chemical Property of 1,4-Pentanediamine, N4-(6-methoxy-4,5-dimethyl-8-quinolinyl)-, (2Z)-2-butenedioate (1:1)

Chemical Property:

Vapor Pressure:3.79E-09mmHg at 25°C
Boiling Point:473.9°Cat760mmHg
Flash Point:240.4°C
Density:g/cm³
Hydrogen Bond Donor Count:4
Hydrogen Bond Acceptor Count:8
Rotatable Bond Count:8
Exact Mass:403.21072103
Heavy Atom Count:29
Complexity:431

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC1=C2C(=C(C=C(C2=NC=C1)NC(C)CCCN)OC)C.C(=CC(=O)O)C(=O)O
Isomeric SMILES:CC1=C2C(=C(C=C(C2=NC=C1)NC(C)CCCN)OC)C.C(=C\C(=O)O)\C(=O)O

Technology Process of 1,4-Pentanediamine, N4-(6-methoxy-4,5-dimethyl-8-quinolinyl)-, (2Z)-2-butenedioate (1:1)

There total 8 articles about 1,4-Pentanediamine, N4-(6-methoxy-4,5-dimethyl-8-quinolinyl)-, (2Z)-2-butenedioate (1:1) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 59353-62-7
4-bromo-1-phthalimidopentane

: 76100-57-7
4,5-dimethyl-6-methoxy-8-<(4-amino-1-methylbutyl)amino>quinoline maleate

Guidance literature:: Multi-step reaction with 2 steps

1: Et₃N / 11 h / 110 - 135 °C

2: 1.) N₂H₄*H₂O / 1.) EtOH, reflux, 3 h

With hydrazine hydrate; triethylamine;
DOI:10.1002/jps.2600690818

Reference yield:

: 446-20-8
5-fluoro-4-methoxy-2-nitroaniline

: 76100-57-7
4,5-dimethyl-6-methoxy-8-<(4-amino-1-methylbutyl)amino>quinoline maleate

Guidance literature:: Multi-step reaction with 6 steps

1: AsO₅, H₃PO₄ / 1.5 h / 85 - 95 °C

2: 87 percent / NaH, copper(I) bromide, 18-crown-6 ether / 6 h / 60 - 80 °C

3: 83.7 percent / AcOH, conc. H₂SO₄ / H₂O / 4 h / Heating

4: 63.6 percent / stannous chloride hydrate, conc HCl / 1.= 0 deg C, 15 min, 2.) room temperature, 5 h

5: Et₃N / 11 h / 110 - 135 °C

6: 1.) N₂H₄*H₂O / 1.) EtOH, reflux, 3 h

With hydrogenchloride; arsenic(V) oxide; 18-crown-6 ether; phosphoric acid; sulfuric acid; sodium hydride; hydrazine hydrate; acetic acid; triethylamine; tin(ll) chloride; copper(I) bromide; In water;
DOI:10.1002/jps.2600690818

Reference yield:

: 64993-12-0
4-methyl-5-fluoro-6-methoxy-8-nitroquinoline

: 76100-57-7
4,5-dimethyl-6-methoxy-8-<(4-amino-1-methylbutyl)amino>quinoline maleate

Guidance literature:: Multi-step reaction with 5 steps

1: 87 percent / NaH, copper(I) bromide, 18-crown-6 ether / 6 h / 60 - 80 °C

2: 83.7 percent / AcOH, conc. H₂SO₄ / H₂O / 4 h / Heating

3: 63.6 percent / stannous chloride hydrate, conc HCl / 1.= 0 deg C, 15 min, 2.) room temperature, 5 h

4: Et₃N / 11 h / 110 - 135 °C

5: 1.) N₂H₄*H₂O / 1.) EtOH, reflux, 3 h

With hydrogenchloride; 18-crown-6 ether; sulfuric acid; sodium hydride; hydrazine hydrate; acetic acid; triethylamine; tin(ll) chloride; copper(I) bromide; In water;
DOI:10.1002/jps.2600690818