triphenylstannanylium piperidine-1-carbodithioate

Base Information

• Chemical Name: triphenylstannanylium piperidine-1-carbodithioate
• CAS No.: 59086-70-3
• Molecular Formula: C24H25NS2Sn
• Molecular Weight: 510.302
• Mol file: 59086-70-3.mol

Synonyms:

Chemical Property of triphenylstannanylium piperidine-1-carbodithioate

Chemical Property:

• Boiling Point: °Cat760mmHg
• Flash Point: °C
• Density: g/cm³

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of triphenylstannanylium piperidine-1-carbodithioate

There total 2 articles about triphenylstannanylium piperidine-1-carbodithioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

triphenyltin chloride (639-58-7) + sodium piperidinedithiocarbamate (873-57-4) → (C6H5)3Sn(SCSN(CH2)5) (59086-70-3)

Guidance literature:

In benzene; byproducts: NaCl; Sn-salt soln. addn. dropwise to org. compd. suspn., mixt. stirring at room temp. for 4 h, refluxing for 6 h, NaCl filtration off, solvent removal from filtrate under reduced pressure; residue recrystn. from chloroform/hexane; elem. anal.;

DOI:10.1080/10426509608046344

Reference yield:

→ triphenyl tin piperidyl dithiocarbamate (59086-70-3)

Guidance literature:

Bis-triphenylzinnoxid, CS2, Piperidin;

DOI:10.1016/S0022-328X(00)91774-1

upstream raw materials:

triphenyltin chloride

sodium piperidinedithiocarbamate

Refernces

• 1、 Sharma, Jyoti,Singh, Yashpal,Rai, Audhesh Kumar. "Synthesis and spectroscopic characterization of heterocyclic dithiocarbamate complexes of triorganotin (IV)". . p. 19 - 26. Retrieved 2007/10/03.