1,1,1-Trimethyl-N-[2,4,6-tri(propan-2-yl)phenyl]silanamine

Base Information

Chemical Name:1,1,1-Trimethyl-N-[2,4,6-tri(propan-2-yl)phenyl]silanamine
CAS No.:70848-22-5
Molecular Formula:C18H33NSi
Molecular Weight:291.54700
Hs Code.:
DSSTox Substance ID:DTXSID20563526
Wikidata:Q82447977

Synonyms:70848-22-5;DTXSID20563526;1,1,1-Trimethyl-N-[2,4,6-tri(propan-2-yl)phenyl]silanamine;AKOS032949288

Suppliers and Price of 1,1,1-Trimethyl-N-[2,4,6-tri(propan-2-yl)phenyl]silanamine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,1,1-Trimethyl-N-[2,4,6-tri(propan-2-yl)phenyl]silanamine

Chemical Property:

PSA：12.03000
LogP:6.37660
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:5
Exact Mass:291.238226591
Heavy Atom Count:20
Complexity:272

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(C)C1=CC(=C(C(=C1)C(C)C)N[Si](C)(C)C)C(C)C

Technology Process of 1,1,1-Trimethyl-N-[2,4,6-tri(propan-2-yl)phenyl]silanamine

There total 5 articles about 1,1,1-Trimethyl-N-[2,4,6-tri(propan-2-yl)phenyl]silanamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

: 75-77-4
chloro-trimethyl-silane

: 21524-36-7
2,4,6-triisopropylaniline

: 70848-22-5
N-trimethylsilyl-1-amino-2,4,6-triisopropylbenzene

Guidance literature:: 2,4,6-triisopropylaniline; With n-butyllithium; In diethyl ether; hexane; at -60 ℃; for 0.5h; Inert atmosphere; Schlenk technique;

chloro-trimethyl-silane; In diethyl ether; at 20 ℃; for 2h;
DOI:10.1039/c6dt00229c

Reference yield:

: 717-74-8
1,3,5-triisopropyl benzene

: 70848-22-5
N-trimethylsilyl-1-amino-2,4,6-triisopropylbenzene

Guidance literature:: Multi-step reaction with 4 steps

1.1: nitric acid / acetic acid; acetic anhydride / 2 h / Inert atmosphere; Schlenk technique

2.1: lithium aluminium tetrahydride / tetrahydrofuran; diethyl ether / 2 h / Reflux; Inert atmosphere; Schlenk technique

3.1: sodium hydroxide / water; pentane / Inert atmosphere; Schlenk technique

4.1: n-butyllithium / hexane; diethyl ether / 0.5 h / -60 °C / Inert atmosphere; Schlenk technique

4.2: 2 h / 20 °C

With lithium aluminium tetrahydride; n-butyllithium; nitric acid; sodium hydroxide; In tetrahydrofuran; diethyl ether; hexane; water; acetic anhydride; acetic acid; pentane;
DOI:10.1039/c6dt00229c

Reference yield:

: 13402-31-8
1,3,5-triisopropyl-2-nitrobenzene

: 70848-22-5
N-trimethylsilyl-1-amino-2,4,6-triisopropylbenzene

Guidance literature:: Multi-step reaction with 3 steps

1.1: lithium aluminium tetrahydride / tetrahydrofuran; diethyl ether / 2 h / Reflux; Inert atmosphere; Schlenk technique

2.1: sodium hydroxide / water; pentane / Inert atmosphere; Schlenk technique

3.1: n-butyllithium / hexane; diethyl ether / 0.5 h / -60 °C / Inert atmosphere; Schlenk technique

3.2: 2 h / 20 °C

With lithium aluminium tetrahydride; n-butyllithium; sodium hydroxide; In tetrahydrofuran; diethyl ether; hexane; water; pentane;
DOI:10.1039/c6dt00229c