Methyl 2-chloro-3-(4-methoxyphenyl)prop-2-enoate

Base Information

Chemical Name:Methyl 2-chloro-3-(4-methoxyphenyl)prop-2-enoate
CAS No.:71481-00-0
Molecular Formula:C₁₁H₁₁ClO₃
Molecular Weight:226.66
Hs Code.:
DSSTox Substance ID:DTXSID20706052

Synonyms:Methyl 2-chloro-3-(4-methoxyphenyl)prop-2-enoate;71481-00-0;DTXSID20706052;methyl 2-chloro-3-p-methoxyphenylacrylate

Suppliers and Price of Methyl 2-chloro-3-(4-methoxyphenyl)prop-2-enoate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Methyl 2-chloro-3-(4-methoxyphenyl)prop-2-enoate

Chemical Property:

XLogP3:3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:4
Exact Mass:226.0396719
Heavy Atom Count:15
Complexity:242

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=CC=C(C=C1)C=C(C(=O)OC)Cl

Technology Process of Methyl 2-chloro-3-(4-methoxyphenyl)prop-2-enoate

There total 10 articles about Methyl 2-chloro-3-(4-methoxyphenyl)prop-2-enoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 598-99-2
Methyl trichloroacetate

: 123-11-5
4-methoxy-benzaldehyde

: 71481-00-0,119555-96-3
(Z)-2-chloro-3-(4-methoxyphenyl)acrylic acid methyl ester

Guidance literature:: With chromium dichloride; In tetrahydrofuran; at 20 ℃; for 0.5h;
DOI:10.1021/ja029938d

Reference yield: 98.0%

: 123-11-5
4-methoxy-benzaldehyde

: 96-34-4
methyl chloroacetate

: 71481-00-0,119555-96-3
(Z)-2-chloro-3-(4-methoxyphenyl)acrylic acid methyl ester

Guidance literature:: 4-methoxy-benzaldehyde; methyl chloroacetate; With titanium tetrachloride; In dichloromethane; at 20 ℃; for 0.666667h; Inert atmosphere;

With triethylamine; In dichloromethane; at 20 - 30 ℃; stereoselective reaction; Inert atmosphere;
DOI:10.1039/c3ob41592a