Benzaldehyde, 4-methoxy-, (6-chloro-3-pyridazinyl)hydrazone

Base Information

• Chemical Name: Benzaldehyde, 4-methoxy-, (6-chloro-3-pyridazinyl)hydrazone
• CAS No.: 7190-95-6
• Molecular Formula: C12H11ClN4O
• Molecular Weight: 262.699

Synonyms:N-(6-Chloro-pyridazin-3-yl)-N'-[1-(4-methoxy-phenyl)-meth-(E)-ylidene]-hydrazine;4-methoxy-benzaldehyde (6-chloro-pyridazin-3-yl)-hydrazone;4-methoxybenzylidene-(6-chloro-3-pyridazinyl)-hydrazine;(4-Methoxybenzaldehyd)-(6-chlorpyridazinyl-3-hydrazon);

Chemical Property of Benzaldehyde, 4-methoxy-, (6-chloro-3-pyridazinyl)hydrazone

Chemical Property:

• Melting Point: 260 - 263 °C (isopropyl alcohol)
• PSA: 59.40000
• LogP: 2.65760

Purity/Quality:

95% ^*data from raw suppliers

Safty Information:

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Technology Process of Benzaldehyde, 4-methoxy-, (6-chloro-3-pyridazinyl)hydrazone

There total 2 articles about Benzaldehyde, 4-methoxy-, (6-chloro-3-pyridazinyl)hydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

3-Chloro-6-hydrazinopyridazine (17284-97-8) + 4-methoxy-benzaldehyde (123-11-5) → 3-[2-(4-methoxybenzylidene)hydrazinyl]-6-chloropyridazine (7190-95-6)

Guidance literature:

In ethanol; for 0.5h; Reflux;

DOI:10.1016/j.bioorg.2019.01.049

Reference yield:

→ 3-[2-(4-methoxybenzylidene)hydrazinyl]-6-chloropyridazine (7190-95-6)

Guidance literature:

6-Chlor-3-hydrazinopyridazin, 4-Methoxy-benzaldehyd;

DOI:10.1016/S0040-4020(01)82127-X

Reference yield: 88.0%

3-[2-(4-methoxybenzylidene)hydrazinyl]-6-chloropyridazine (7190-95-6) → 6-chloro-3-(4'-methoxyphenyl)-[1,2,4]triazolo[4,3-b]pyridazine (7190-82-1)

Guidance literature:

With [bis(acetoxy)iodo]benzene; In dichloromethane; at 20 ℃;

DOI:10.1016/j.bioorg.2019.01.049

upstream raw materials:

3-Chloro-6-hydrazinopyridazine

4-methoxy-benzaldehyde

Downstream raw materials:

6-chloro-3-(4'-methoxyphenyl)-[1,2,4]triazolo[4,3-b]pyridazine

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