3,6-Dibromo-9-(4-bromophenyl)-9H-carbazole

Base Information

• Chemical Name: 3,6-Dibromo-9-(4-bromophenyl)-9H-carbazole
• CAS No.: 73087-83-9
• Molecular Formula: C18H10Br3N
• Molecular Weight: 479.996
• Hs Code.: 2933990090
• European Community (EC) Number: 808-076-4
• DSSTox Substance ID: DTXSID60453674
• Nikkaji Number: J620.142C
• Wikidata: Q82274873
• Mol file: 73087-83-9.mol

Synonyms:3,6-Dibromo-9-(4-bromophenyl)-9H-carbazole;73087-83-9;3,6-dibromo-9-(4-bromophenyl)carbazole;9-(4-Bromophenyl)-3,6-dibromo-9H-carbazole;9H-Carbazole, 3,6-dibromo-9-(4-bromophenyl)-;C18H10Br3N;3,6-Dibromo-9-(4-bromo-phenyl)-9H-carbazole;YSWG315;SCHEMBL782332;DTXSID60453674;AMY19413;YCA08783;MFCD12024284;AKOS016010691;DS-5671;3,6-dibromo-9-(p-bromophenyl)carbazole;CS-0098887;D4563;A866153

Chemical Property of 3,6-Dibromo-9-(4-bromophenyl)-9H-carbazole

Chemical Property:

• Melting Point: 207.0 to 211.0 °C
• Boiling Point: 538.2±50.0 °C(Predicted)
• PSA: 4.93000
• Density: 1.86±0.1 g/cm3(Predicted)
• LogP: 7.07120
• Storage Temp.: Sealed in dry,Room Temperature
• XLogP3: 7.1
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 0
• Rotatable Bond Count: 1
• Exact Mass: 478.83429
• Heavy Atom Count: 22
• Complexity: 370

Purity/Quality:

97% ^*data from raw suppliers

3,6-Dibromo-9-(4-bromophenyl)-9H-carbazole ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: C1=CC(=CC=C1N2C3=C(C=C(C=C3)Br)C4=C2C=CC(=C4)Br)Br

Technology Process of 3,6-Dibromo-9-(4-bromophenyl)-9H-carbazole

There total 18 articles about 3,6-Dibromo-9-(4-bromophenyl)-9H-carbazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

N-(4-bromophenyl)carbazole (57102-42-8) → 3,6-dibromo-9-(4-bromophenyl)-9H-carbazole (73087-83-9)

Guidance literature:

With N-Bromosuccinimide; In dichloromethane; at 0 ℃; for 16h; Schlenk technique; Darkness; Inert atmosphere;

DOI:10.1039/c6ob00140h

Reference yield: 85.2%

N-phenylcarbazole (1150-62-5) → 3,6-dibromo-9-(4-bromophenyl)-9H-carbazole (73087-83-9)

Guidance literature:

With hydrogen bromide; dihydrogen peroxide; In dichloromethane; at 20 ℃; for 4h; Reagent/catalyst; Solvent;

Reference yield: 83.0%

toluene (108-88-3,15644-74-3,16713-13-6) → 1-methyl-4-(phenylmethyl)benzene (620-83-7) + 2-benzyltoluene (713-36-0) + tri(p-bromophenyl)amine (4316-58-9) + 3,6-dibromo-9-(4-bromophenyl)-9H-carbazole (73087-83-9)

Guidance literature:

With tris-(4-bromophenyl)aminium hexachloroantimonate; In dichloromethane; Title compound not separated from byproducts; Irradiation;

DOI:10.1021/jo00103a069

upstream raw materials:

N-phenylcarbazole

tri(p-bromophenyl)amine

tris(p-bromophenyl)amine radical cation

toluene

Downstream raw materials:

3,6-bis(diphenylphosphonyl)-9-[4-(diphenylphosphonyl)phenyl]-9H-carbazole

C₅₄H₄₀NP₃

9-(phenylboronic-4-yl)-9H-carbazole-3,6-diboronic acid

3,6-bis(bis(2,4,6-trimethylphenyl)boranyl)-9-(4-(bis(2,4,6-trimethylphenyl)boranyl)phenyl)carbazole

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