Pyridazine, 4-[(1E)-2-(4-methoxyphenyl)ethenyl]-

Base Information

Chemical Name:Pyridazine, 4-[(1E)-2-(4-methoxyphenyl)ethenyl]-
CAS No.:73477-02-8
Molecular Formula:C13H12N2O
Molecular Weight:212.251
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Pyridazine, 4-[(1E)-2-(4-methoxyphenyl)ethenyl]-

Chemical Property:

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Safty Information:

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MSDS Files:: SDS file from LookChem

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Technology Process of Pyridazine, 4-[(1E)-2-(4-methoxyphenyl)ethenyl]-

There total 6 articles about Pyridazine, 4-[(1E)-2-(4-methoxyphenyl)ethenyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 185848-13-9
1-(4-methoxyphenyl)-2-(4-pyridazinyl)ethanol

: 73477-02-8
(E)-4-<2-(4-methoxyphenyl)ethenyl>pyridazine

Guidance literature:: With hydrogenchloride; In methanol; for 7h; Heating;
DOI:10.1016/0040-4020(94)01050-A

Reference yield: 72.0%

: 1120-88-3
4-methylpyridazine

: 123-11-5
4-methoxy-benzaldehyde

: 73477-02-8
(E)-4-<2-(4-methoxyphenyl)ethenyl>pyridazine

Guidance literature:: With sodium hydroxide; In dimethyl sulfoxide; for 5h; Ambient temperature;
DOI:10.1002/ardp.19803130111

Reference yield:

: 5754-18-7
4-methyl-1,2-dihydropyridazine-3,6-dione

: 73477-02-8
(E)-4-<2-(4-methoxyphenyl)ethenyl>pyridazine

Guidance literature:: Multi-step reaction with 3 steps

1: POCl₃

2: palladium/charcoal; aq.-ethanolic NH₃ / Hydrogenation

3: 150 °C

With palladium on activated charcoal; ammonia; trichlorophosphate;
DOI:10.1021/ja01637a051