Carbamic acid, (5-bromo-2-chlorophenyl)-, 1,1-dimethylethyl ester

Base Information

Chemical Name:Carbamic acid, (5-bromo-2-chlorophenyl)-, 1,1-dimethylethyl ester
CAS No.:740806-51-3
Molecular Formula:C11H13BrClNO2
Molecular Weight:306.587
Hs Code.:

Synonyms:(5-bromo-2-chloro-phenyl)-carbamic acid tert-butyl ester;tert-butyl 5-bromo-2-chlorophenylcarbamate;

Suppliers and Price of Carbamic acid, (5-bromo-2-chlorophenyl)-, 1,1-dimethylethyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 5 raw suppliers

Chemical Property of Carbamic acid, (5-bromo-2-chlorophenyl)-, 1,1-dimethylethyl ester

Chemical Property:

Melting Point:84.5 - 85.6 °C
Boiling Point:299.9±30.0 °C(Predicted)
PSA：38.33000
Density:1.484±0.06 g/cm3(Predicted)
LogP:4.52250

Purity/Quality:: 97% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

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Technology Process of Carbamic acid, (5-bromo-2-chlorophenyl)-, 1,1-dimethylethyl ester

There total 6 articles about Carbamic acid, (5-bromo-2-chlorophenyl)-, 1,1-dimethylethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 24424-99-5
di-tert-butyl dicarbonate

: 60811-17-8
5-bromo-2-chloroaniline

: 740806-51-3
tert-butyl (5-bromo-2-chlorophenyl)carbamate

Guidance literature:: With dmap; triethylamine; In dichloromethane; at 0 - 20 ℃;

Reference yield: 85.0%

: 21739-92-4
5-bromo-2-chlorobenzoic acid

: 75-65-0
tert-butyl alcohol

: 740806-51-3
tert-butyl (5-bromo-2-chlorophenyl)carbamate

Guidance literature:: With diphenyl phosphoryl azide; triethylamine; for 3h; Heating / reflux;

Reference yield: 69.0%

: 25216-74-4
tert-butyl (3-bromophenyl)carbamate

: 740806-51-3
tert-butyl (5-bromo-2-chlorophenyl)carbamate

Guidance literature:: With 1,3-dichloro-5,5-dimethylhydantoin; diisopropylamine hydrochloride; In toluene; at 25 ℃; for 14h; regioselective reaction; Darkness; Green chemistry;
DOI:10.1002/anie.201607388