DL-Phenylalanine, N-benzoyl-, methyl ester

Base Information

• Chemical Name: DL-Phenylalanine, N-benzoyl-, methyl ester
• CAS No.: 74923-17-4
• Molecular Formula: C17H17NO3
• Molecular Weight: 283.327
• Mol file: 74923-17-4.mol

Synonyms:

Chemical Property of DL-Phenylalanine, N-benzoyl-, methyl ester

Chemical Property:

Purity/Quality:

90% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of DL-Phenylalanine, N-benzoyl-, methyl ester

There total 29 articles about DL-Phenylalanine, N-benzoyl-, methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

methyl (Z)-2-benzoylamino-3-phenyl-2-propenoate (21462-02-2) → methyl N-benzoylphenylalaninate (74923-17-4)

Guidance literature:

With hydrogen; for 0.00277778h;

DOI:10.1021/acs.jpca.5b06802

Reference yield: 95.0%

methanol (67-56-1) + 2-Benzoylamino-3-phenyl-propionic acid prop-2-ynyl ester (92136-48-6) → methyl N-benzoylphenylalaninate (74923-17-4)

Guidance literature:

With ammonium cerium(IV) nitrate; at 20 ℃; for 54h;

DOI:10.1081/SCC-120004264

Reference yield: 94.0%

DL-phenylalanine methyl ester (15028-44-1) + benzoyl chloride (98-88-4) → methyl N-benzoylphenylalaninate (74923-17-4)

Guidance literature:

With P₂W₁₈O₆₂^(6-)*6H⁽¹⁺⁾*14H₂O; In neat (no solvent); at 20 ℃; for 0.0333333h; Green chemistry;

DOI:10.1080/00304948.2021.1877238

upstream raw materials:

methyl ester of benzoylaminocinnamic acid

DL-phenylalanine methyl ester

benzoyl chloride

diazomethane

Downstream raw materials:

N-benzoylphenylalanine ethylester

N-[3-benzyltetrahydro-2-oxofuran-3-yl]benzamide

N-benzoyl-L-phenylalanine

methyl (R)-2-(benzoylamino)-3-phenylpropanoate