3'-Adenylic acid, N-benzoyl-2'-O-[(1,1-dimethylethyl)dimethylsilyl]-5'-O-[(4-methoxyphenyl )diphenylmethyl]-, 2-chlorophenyl 2-cyanoethyl ester

Base Information

Chemical Name:3'-Adenylic acid, N-benzoyl-2'-O-[(1,1-dimethylethyl)dimethylsilyl]-5'-O-[(4-methoxyphenyl )diphenylmethyl]-, 2-chlorophenyl 2-cyanoethyl ester
CAS No.:75085-66-4
Molecular Formula:C52H54ClN6O9PSi
Molecular Weight:1001.55
Hs Code.:

3'-Adenylic acid,
N-benzoyl-2'-O-[(1,1-dimethylethyl)dimethylsilyl]-5'-O-[(4-methoxyphenyl
)diphenylmethyl]-, 2-chlorophenyl 2-cyanoethyl ester

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3'-Adenylic acid, N-benzoyl-2'-O-[(1,1-dimethylethyl)dimethylsilyl]-5'-O-[(4-methoxyphenyl )diphenylmethyl]-, 2-chlorophenyl 2-cyanoethyl ester

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 3'-Adenylic acid, N-benzoyl-2'-O-[(1,1-dimethylethyl)dimethylsilyl]-5'-O-[(4-methoxyphenyl )diphenylmethyl]-, 2-chlorophenyl 2-cyanoethyl ester

There total 7 articles about 3'-Adenylic acid, N-benzoyl-2'-O-[(1,1-dimethylethyl)dimethylsilyl]-5'-O-[(4-methoxyphenyl )diphenylmethyl]-, 2-chlorophenyl 2-cyanoethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 69504-00-3
N⁶-Benzoyl-5'-O-(monomethoxytrityl)adenosine

: 75085-66-4
N⁶-Benzoyl-2'-O-t-butyldimethylsilyl-5'-monomethoxytrityladenosin-3'-(β-cyanoaethyl)(o-chlorphenyl)phosphat

Guidance literature:: Multi-step reaction with 3 steps

1: 36 percent / imidazole / pyridine

2: pyridine

With 1H-imidazole; In pyridine;
DOI:10.1016/S0040-4039(00)93649-9

Reference yield:

: 18162-48-6
tert-butyldimethylsilyl chloride

: 75085-66-4
N⁶-Benzoyl-2'-O-t-butyldimethylsilyl-5'-monomethoxytrityladenosin-3'-(β-cyanoaethyl)(o-chlorphenyl)phosphat

Guidance literature:: Multi-step reaction with 3 steps

1: 36 percent / imidazole / pyridine

2: pyridine

With 1H-imidazole; In pyridine;
DOI:10.1016/S0040-4039(00)93649-9

Reference yield:

: 72351-28-1
2-chlorophenyl phosphordi(1H-1-[1,2,4]triazolide)

: 75085-66-4
N⁶-Benzoyl-2'-O-t-butyldimethylsilyl-5'-monomethoxytrityladenosin-3'-(β-cyanoaethyl)(o-chlorphenyl)phosphat

Guidance literature:: Multi-step reaction with 2 steps

1: N-methylimidazole / pyridine / 0.17 h / -20 °C

2: pyridine / 5 h / Ambient temperature

With 1-methyl-1H-imidazole; In pyridine;
DOI:10.1002/hlca.19810640548