2-cyanoethyl piperidine-1-carbodithioate

Base Information

• Chemical Name: 2-cyanoethyl piperidine-1-carbodithioate
• CAS No.: 33032-83-6
• Molecular Formula: C9H14N2S2
• Molecular Weight: 214.3509
• Mol file: 33032-83-6.mol

Synonyms:

Chemical Property of 2-cyanoethyl piperidine-1-carbodithioate

Chemical Property:

• Vapor Pressure: 2.24E-05mmHg at 25°C
• Boiling Point: 360.3°Cat760mmHg
• Flash Point: 171.7°C
• Density: 1.211g/cm³

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-cyanoethyl piperidine-1-carbodithioate

There total 3 articles about 2-cyanoethyl piperidine-1-carbodithioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

piperidine (110-89-4) + carbon disulfide (75-15-0,12122-00-8) + acrylonitrile (107-13-1,25014-41-9) → N,N-Pentamethylen-dithiocarbamidsaeure-S-(2-cyanethylester) (33032-83-6)

Guidance literature:

With 1-pentyl-3-methylimidazolium bromide; at 28 - 30 ℃; for 0.166667h;

DOI:10.1002/ejoc.200700842

Reference yield:

acrylonitrile (107-13-1,25014-41-9) + sodium piperidinedithiocarbamate (873-57-4) → N,N-Pentamethylen-dithiocarbamidsaeure-S-(2-cyanethylester) (33032-83-6)

Guidance literature:

With water;

Reference yield:

→ N,N-Pentamethylen-dithiocarbamidsaeure-S-(2-cyanethylester) (33032-83-6)

Guidance literature:

CS2, Piperidin, Acrylnitril;

DOI:10.1002/ardp.19713040702

upstream raw materials:

acrylonitrile

sodium piperidinedithiocarbamate

piperidine

carbon disulfide

Refernces

• 1、 Azizi, Najmadin,Gholibeglo, Elahm,Nayeri, Sanaz Dehghan. "An efficient synthesis of dithiocarbamates under ultrasound irradiation in water". experimental part. p. 1171 - 1174. Retrieved 2012/09/25.
• 2、 Karmakar, Bikash,Banerji, Julie. "An expedient, fast and competent synthesis of organic dithiocarbamates over nanocrystalline MgO in water at room temperature". experimental part. p. 6584 - 6586. Retrieved 2011/12/22.