5-Chloro-2-iodobenzophenone

Base Information

Chemical Name:5-Chloro-2-iodobenzophenone
CAS No.:76049-48-4
Molecular Formula:C13H8ClIO
Molecular Weight:342.563
Hs Code.:
DSSTox Substance ID:DTXSID40513669
Nikkaji Number:J1.149.916C
Wikidata:Q82373591

Synonyms:5-chloro-2-iodobenzophenone;76049-48-4;5-chloro- 2-iodobenzophenone;SCHEMBL10994311;DTXSID40513669;AQDOLAWKRIYYAT-UHFFFAOYSA-N;(5-Chloro-2-iodophenyl)(phenyl)methanone

Suppliers and Price of 5-Chloro-2-iodobenzophenone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 0 raw suppliers

Chemical Property of 5-Chloro-2-iodobenzophenone

Chemical Property:

XLogP3:4.5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:2
Exact Mass:341.93084
Heavy Atom Count:16
Complexity:250

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)C(=O)C2=C(C=CC(=C2)Cl)I

Technology Process of 5-Chloro-2-iodobenzophenone

There total 6 articles about 5-Chloro-2-iodobenzophenone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 13755-29-8
sodium tetrafluoroborate

: 719-59-5
5-chloro-2-aminobenzophenone

: 76049-48-4
5-chloro-2-iodobenzophenone

Guidance literature:: With potassium iodide; sulfuric acid; sodium nitrite; In water; Petroleum ether;

Reference yield:

: 150879-48-4
N-methyl-N-methyloxy-2-amino-5-chlorobenzamide

: 76049-48-4
5-chloro-2-iodobenzophenone

Guidance literature:: Multi-step reaction with 2 steps

1: n-butyllithium / tetrahydrofuran; hexane / 0.5 h / -78 °C / Inert atmosphere

2: toluene-4-sulfonic acid; sodium nitrite; potassium iodide / water; acetonitrile / 2 h / 25 °C

With n-butyllithium; toluene-4-sulfonic acid; potassium iodide; sodium nitrite; In tetrahydrofuran; hexane; water; acetonitrile;
DOI:10.1021/acs.orglett.8b01812

Reference yield:

: 108-86-1,52753-63-6
bromobenzene

: 76049-48-4
5-chloro-2-iodobenzophenone

Guidance literature:: Multi-step reaction with 2 steps

1: n-butyllithium / tetrahydrofuran; hexane / 0.5 h / -78 °C / Inert atmosphere

2: toluene-4-sulfonic acid; sodium nitrite; potassium iodide / water; acetonitrile / 2 h / 25 °C

With n-butyllithium; toluene-4-sulfonic acid; potassium iodide; sodium nitrite; In tetrahydrofuran; hexane; water; acetonitrile;
DOI:10.1021/acs.orglett.8b01812